Technology Process of C18H19NO3S
There total 14 articles about C18H19NO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver hexafluoroantimonate; C27H37AuClN2;
In
dichloromethane;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ol302743k
- Guidance literature:
-
With
silver hexafluoroantimonate; [AuCl(PPh3)3];
In
dichloromethane;
at 20 ℃;
for 60h;
Inert atmosphere;
DOI:10.1021/ol302743k
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / toluene / 24 h / 150 °C / Inert atmosphere
2: dimethyl zinc(II) / toluene; n-heptane; tetrahydrofuran / 70 °C / Inert atmosphere
3: potassium carbonate / acetone / 24 h / 20 °C / Inert atmosphere
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere
5: silver hexafluoroantimonate; C27H37AuClN2 / dichloromethane / 1 h / 20 °C / Inert atmosphere
With
silver hexafluoroantimonate; C27H37AuClN2; tetrabutyl ammonium fluoride; dimethyl zinc(II); potassium carbonate; toluene-4-sulfonic acid;
In
tetrahydrofuran; n-heptane; dichloromethane; acetone; toluene;
5: |Nazarov Cyclization;
DOI:10.1021/ol302743k