(R)-4-((R)-(4-methoxyphenyl)((2-phenylallyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolane

Base Information

Chemical Name:(R)-4-((R)-(4-methoxyphenyl)((2-phenylallyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolane
CAS No.:1022915-05-4
Molecular Formula:C₂₂H₂₆O₄
Molecular Weight:354.446
Hs Code.:

Synonyms:(R)-4-((R)-(4-methoxyphenyl)((2-phenylallyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-4-((R)-(4-methoxyphenyl)((2-phenylallyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolane

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Technology Process of (R)-4-((R)-(4-methoxyphenyl)((2-phenylallyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolane

There total 3 articles about (R)-4-((R)-(4-methoxyphenyl)((2-phenylallyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 3360-54-1
3-bromo-2-phenylprop-1-ene

: 102389-96-8
(2R,3R)-3-hydroxy-1,2-O-isopropylidene-3-p-methoxyphenyl-1,2-propanediol

: 1022915-05-4
(R)-4-((R)-(4-methoxyphenyl)((2-phenylallyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolane

Guidance literature:: (2R,3R)-3-hydroxy-1,2-O-isopropylidene-3-p-methoxyphenyl-1,2-propanediol; With sodium hydride; In mineral oil; at 55 ℃; for 0.5h;

3-bromo-2-phenylprop-1-ene; In mineral oil; at 0 ℃; for 5h; Reflux;
DOI:10.1055/s-0033-1340163

Reference yield:

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 1022915-05-4
(R)-4-((R)-(4-methoxyphenyl)((2-phenylallyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

1.3: pH 9 / Inert atmosphere

2.1: sodium hydride / mineral oil / 0.5 h / 55 °C

2.2: 5 h / 0 °C / Reflux

With copper(l) iodide; sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1055/s-0033-1340163

Reference yield:

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 1022915-05-4
(R)-4-((R)-(4-methoxyphenyl)((2-phenylallyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

1.3: pH 9 / Inert atmosphere

2.1: sodium hydride / mineral oil / 0.5 h / 55 °C

2.2: 5 h / 0 °C / Reflux

With copper(l) iodide; sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1055/s-0033-1340163