N-Methyl 5-bromopicolinamide

Base Information

Chemical Name:N-Methyl 5-bromopicolinamide
CAS No.:845305-87-5
Molecular Formula:C7H7BrN2O
Molecular Weight:215.049
Hs Code.:2933399090
Mol file:845305-87-5.mol

Synonyms:5-Bromo-N-methylpyridine-2-carboxamide;N-Methyl 5-bromopicolinamide;N-methyl 5-bromopyridine-2-carboxamide

Suppliers and Price of N-Methyl 5-bromopicolinamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
5-Bromo-N-methylpyridine-2-carboxamide
10g
$ 691.00

Alfa Aesar
5-Bromo-N-methylpyridine-2-carboxamide, 96%
250mg
$ 34.00

Alfa Aesar
5-Bromo-N-methylpyridine-2-carboxamide, 96%
1g
$ 113.00

Alfa Aesar
5-Bromo-N-methylpyridine-2-carboxamide, 96%
5g
$ 456.00

Alichem
5-Bromo-N-methylpicolinamide
10g
$ 496.65

Ambeed
5-Bromo-N-methylpicolinamide 98%
1g
$ 97.00

Ambeed
5-Bromo-N-methylpicolinamide 98%
5g
$ 165.00

Ambeed
5-Bromo-N-methylpicolinamide 98%
100mg
$ 16.00

Ambeed
5-Bromo-N-methylpicolinamide 98%
250mg
$ 23.00

Ambeed
5-Bromo-N-methylpicolinamide 98%
25g
$ 1216.00

Total 26 raw suppliers

Chemical Property of N-Methyl 5-bromopicolinamide

Chemical Property:

Vapor Pressure:5.62E-05mmHg at 25°C
Melting Point:76-77℃
Refractive Index:1.569
Boiling Point:346.8ºC at 760 mmHg
PKA:13.54±0.46(Predicted)
Flash Point:163.5ºC
PSA：41.99000
Density:1.545g/cm3
LogP:1.59460
Storage Temp.:Inert atmosphere,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

5-Bromo-N-methylpyridine-2-carboxamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Methyl 5-bromopicolinamide

There total 1 articles about N-Methyl 5-bromopicolinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 29682-15-3
methyl 5-bromopicolinate

: 74-89-5
methylamine

: 845305-87-5
5-bromo-2-(N-methylaminocarbonyl)pyridine

Guidance literature:: In tetrahydrofuran; at 20 ℃;

Reference yield: 98.0%

: 80460-73-7
(4-aminophenyl)boronic acid hydrochloride

: 845305-87-5
5-bromo-2-(N-methylaminocarbonyl)pyridine

: 5-(4-aminophenyl)-N-methylpyridine-2-carboxamide

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,4-dioxane; water; at 100 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2015.04.071

Reference yield: 68.2%

: 845305-87-5
5-bromo-2-(N-methylaminocarbonyl)pyridine

: C₁₃H₁₄N₄O₃S

: 5-(1-((4-aminocarbonylphenyl)sulfonyl)-1,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridin-6-yl)-N-methyl-2-pyridinecarboxamide

Guidance literature:: With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; In toluene; at 100 ℃; for 12h;