N-(but-3-enyl)-N-{(1S)-1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-enyl}-4-methoxybenzylamine

Base Information

Chemical Name:N-(but-3-enyl)-N-{(1S)-1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-enyl}-4-methoxybenzylamine
CAS No.:262284-60-6
Molecular Formula:C₂₀H₂₉NO₃
Molecular Weight:331.455
Hs Code.:

Synonyms:N-(but-3-enyl)-N-{(1S)-1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-enyl}-4-methoxybenzylamine

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Chemical Property of N-(but-3-enyl)-N-{(1S)-1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-enyl}-4-methoxybenzylamine

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Technology Process of N-(but-3-enyl)-N-{(1S)-1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-enyl}-4-methoxybenzylamine

There total 4 articles about N-(but-3-enyl)-N-{(1S)-1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-enyl}-4-methoxybenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 5162-44-7
1-bromo-4-butene

: 262284-59-3
N-{(1S)-1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-enyl}-4-methoxybenzylamine

: 262284-60-6
N-(but-3-enyl)-N-{(1S)-1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-enyl}-4-methoxybenzylamine

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 100 ℃;

Reference yield:

: 124455-21-6,124455-24-9
[1-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-meth-(E)-ylidene]-(4-methoxy-benzyl)-amine

: 262284-60-6
N-(but-3-enyl)-N-{(1S)-1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-enyl}-4-methoxybenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / diethyl ether; tetrahydrofuran / 20 °C

2: 74 percent / K₂CO₃; NaI; nBu₄NI / dimethylformamide / 15 h / 70 °C

With tetra-(n-butyl)ammonium iodide; potassium carbonate; sodium iodide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/1099-0690(200108)2001:15<2841::AID-EJOC2841>3.0.CO;2-W

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 262284-60-6
N-(but-3-enyl)-N-{(1S)-1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]prop-2-enyl}-4-methoxybenzylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / MgSO₄ / diethyl ether / 3 h / 0 °C

2: 84 percent / diethyl ether; tetrahydrofuran / 20 °C

3: 74 percent / K₂CO₃; NaI; nBu₄NI / dimethylformamide / 15 h / 70 °C

With tetra-(n-butyl)ammonium iodide; magnesium sulfate; potassium carbonate; sodium iodide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/1099-0690(200108)2001:15<2841::AID-EJOC2841>3.0.CO;2-W