tris(benzyloxy)-4,6,6'-dichloro-3,3'-methoxy-4'-dimethyl-2,2'-benzophenone

Base Information

Chemical Name:tris(benzyloxy)-4,6,6'-dichloro-3,3'-methoxy-4'-dimethyl-2,2'-benzophenone
CAS No.:98968-82-2
Molecular Formula:C₃₇H₃₂Cl₂O₅
Molecular Weight:627.564
Hs Code.:

Synonyms:tris(benzyloxy)-4,6,6'-dichloro-3,3'-methoxy-4'-dimethyl-2,2'-benzophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris(benzyloxy)-4,6,6'-dichloro-3,3'-methoxy-4'-dimethyl-2,2'-benzophenone

Chemical Property:

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Technology Process of tris(benzyloxy)-4,6,6'-dichloro-3,3'-methoxy-4'-dimethyl-2,2'-benzophenone

There total 7 articles about tris(benzyloxy)-4,6,6'-dichloro-3,3'-methoxy-4'-dimethyl-2,2'-benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 68048-05-5
acide bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoique

: 78135-48-5
benzyloxy-5-chloro-2-methoxy-3-toluene

: 98968-82-2
tris(benzyloxy)-4,6,6'-dichloro-3,3'-methoxy-4'-dimethyl-2,2'-benzophenone

Guidance literature:: With trifluoroacetic anhydride; In dichloromethane; for 5h;
DOI:10.1002/hlca.19850680417

Reference yield:

: 3187-58-4
methyl orsellinate

: 98968-82-2
tris(benzyloxy)-4,6,6'-dichloro-3,3'-methoxy-4'-dimethyl-2,2'-benzophenone

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / SOCl₂ / CH₂Cl₂ / 3 h / Heating

2: 69 percent / anh. K₂CO₃ / dimethylformamide / 15 h / 50 °C

3: 92.8 percent / KOH / dimethylsulfoxide / 30 h / 85 °C

4: 80 percent / (CF₃CO)2O / CH₂Cl₂ / 5 h

With potassium hydroxide; thionyl chloride; potassium carbonate; trifluoroacetic anhydride; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19850680417

Reference yield:

: 711-47-7
chloro-3-dihydroxy-4,6-methyl-2-benzoate de methyle

: 98968-82-2
tris(benzyloxy)-4,6,6'-dichloro-3,3'-methoxy-4'-dimethyl-2,2'-benzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / anh. K₂CO₃ / dimethylformamide / 15 h / 50 °C

2: 92.8 percent / KOH / dimethylsulfoxide / 30 h / 85 °C

3: 80 percent / (CF₃CO)2O / CH₂Cl₂ / 5 h

With potassium hydroxide; potassium carbonate; trifluoroacetic anhydride; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19850680417