4,4-difluoro-2,3,6-triiodo-5-(4-methoxyphenylamino)-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indacene

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Chemical Name:4,4-difluoro-2,3,6-triiodo-5-(4-methoxyphenylamino)-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indacene
CAS No.:1354013-70-9
Molecular Formula:C₂₃H₁₇BF₂I₃N₃O
Molecular Weight:780.929
Hs Code.:

Synonyms:4,4-difluoro-2,3,6-triiodo-5-(4-methoxyphenylamino)-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indacene

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Chemical Property of 4,4-difluoro-2,3,6-triiodo-5-(4-methoxyphenylamino)-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 4,4-difluoro-2,3,6-triiodo-5-(4-methoxyphenylamino)-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indacene

There total 2 articles about 4,4-difluoro-2,3,6-triiodo-5-(4-methoxyphenylamino)-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1354013-80-1
4,4-difluoro-2,3,5,6-tetraiodo-8-(4-methylphenyl)-4-bora-3a,4a-diaza-s-indacene

: 104-94-9
4-methoxy-aniline

: 1354013-70-9
4,4-difluoro-2,3,6-triiodo-5-(4-methoxyphenylamino)-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: In acetonitrile; for 8h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2011.11.070

Reference yield:

: 955084-10-3
5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

: 1354013-70-9
4,4-difluoro-2,3,6-triiodo-5-(4-methoxyphenylamino)-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 2 steps

1: Iodine monochloride / methanol; dichloromethane / 6 h / Reflux

2: acetonitrile / 8 h / Reflux; Inert atmosphere

With Iodine monochloride; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2011.11.070

Reference yield: 46.0%

: 1354013-70-9
4,4-difluoro-2,3,6-triiodo-5-(4-methoxyphenylamino)-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indacene

: 87199-17-5
4-formylphenylboronic acid,

: 1354013-78-7
4,4-difluoro-2,3,6-(4-formylphenyl)-5-(4-methoxyphenylamino)-8-(4-tolyl)-4-bora-3a,4a-diaza-s-indecene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; at 75 ℃; for 5h; Sonication;
DOI:10.1016/j.tet.2011.11.070