5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoic acid

Base Information

Chemical Name:5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoic acid
CAS No.:1189351-80-1
Molecular Formula:C₁₆H₁₈N₂O₃S
Molecular Weight:318.397
Hs Code.:

Synonyms:5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoic acid

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Chemical Property of 5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoic acid

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Technology Process of 5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoic acid

There total 1 articles about 5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1189351-76-5
methyl 5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoate

: 1189351-80-1
5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoic acid

Guidance literature:: methyl 5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoate; With water; lithium hydroxide; In tetrahydrofuran; at 100 ℃; for 1h; Microwave irradiation;

With citric acid; In tetrahydrofuran; water; pH=5 - 6;

Reference yield: 55.0%

: 1189351-80-1
5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1189353-20-5
C₁₈H₂₃N₃O₃S

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; water; at 20 ℃; for 3h; pH=4.5;

Reference yield:

: 67-56-1
methanol

: 1189351-80-1
5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoic acid

: 62-53-3
aniline

: 1189351-82-3
C₂₂H₂₃N₃O₂S

: 1189351-83-4
C₂₃H₂₅N₃O₂S

Guidance literature:: 5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoic acid; aniline; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 48h;

methanol;