N,N'-Methanetetraylbis[1-naphthalenamine]

Base Information

• Chemical Name: N,N'-Methanetetraylbis[1-naphthalenamine]
• CAS No.: 742-16-5
• Molecular Formula: C₂₁H₁₄N₂
• Molecular Weight: 294.356
• DSSTox Substance ID: DTXSID701271556
• Nikkaji Number: J3.009.183C

Synonyms:SCHEMBL194924;DTXSID701271556;742-16-5;N,N'-Methanetetraylbis[1-naphthalenamine]

Chemical Property of N,N'-Methanetetraylbis[1-naphthalenamine]

Chemical Property:

• XLogP3: 6.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 294.115698455
• Heavy Atom Count: 23
• Complexity: 407

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC=C2N=C=NC3=CC=CC4=CC=CC=C43

Technology Process of N,N'-Methanetetraylbis[1-naphthalenamine]

There total 1 articles about N,N'-Methanetetraylbis[1-naphthalenamine] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

S-methyl-N,N'-di-[1]naphthyl-isothiourea → methylthiol (74-93-1) + N,N-(1-naphthyl)carbodiimide (742-16-5)

Guidance literature:

bei starkem Erhitzen;

Reference yield: 80.0%

N,N-(1-naphthyl)carbodiimide (742-16-5) + 1-phenyl-propan-1-one (93-55-0) → N-1-naphthalenyl-benzamide (634-42-4)

Guidance literature:

With [{HMn(CO)₄}3]; In 1,4-dioxane; at 135 ℃; for 24h; Sealed tube; Inert atmosphere;

DOI:10.1002/anie.201104704

Reference yield: 63.0%

2-methyl-4,4-diphenylbuta-2,3-dienoic acid (6002-06-8) + N,N-(1-naphthyl)carbodiimide (742-16-5) → (1R*,7R*)-4-methyl-2-(N-(1-naphtyl)carbamoyl)-6,6-diphenyl-2-azabenzo(8,9)tricyclo(5.2.2.0 1,5)undeca-4,8,10-trien-3-one

Guidance literature:

In tetrahydrofuran; for 168h; Ambient temperature;

DOI:10.1002/hlca.19870700130

Downstream raw materials:

C₃₄H₂₅N₃

N-(naphthalen-1-yl)-3-phenylpropiolamide

N-Phenylpropargyl-N,N'-bis-(1-naphthyl)-harnstoff

N,N'-bis(1-naphthyl)thiourea

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