2,2,2-trichloroethyl N-p-tolylcarbamate

Base Information

Chemical Name:2,2,2-trichloroethyl N-p-tolylcarbamate
CAS No.:37934-96-6
Molecular Formula:C₁₀H₁₀Cl₃NO₂
Molecular Weight:282.554
Hs Code.:

Synonyms:2,2,2-trichloroethyl N-p-tolylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2,2-trichloroethyl N-p-tolylcarbamate

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Technology Process of 2,2,2-trichloroethyl N-p-tolylcarbamate

There total 2 articles about 2,2,2-trichloroethyl N-p-tolylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 106-49-0,12221-03-3
p-toluidine

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 37934-96-6
2,2,2-trichloroethyl N-p-tolylcarbamate

Guidance literature:: With pyridine; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jo981816+

Reference yield:

: 931109-52-3
O-tosyl-N-trichloroethoxycarbonylhydroxylamine

: 108-88-3,15644-74-3,16713-13-6
toluene

: 2,2,2-trichloroethyl N-o-tolylcarbamate

: 2,2,2-trichloroethyl N-m-tolylcarbamate

: 37934-96-6
2,2,2-trichloroethyl N-p-tolylcarbamate

Guidance literature:: With tetrakis(acetonitrile)copper(I) hexafluorophosphate; 2.9-dimethyl-1,10-phenanthroline; at 140 ℃; for 8h; Overall yield = 59 %; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3cc46412a