{bis(trimethylsilyl)phosphido}carbonylnitrosyl(pentamethylcyclopentadienyl)rhenium

Base Information

Chemical Name:{bis(trimethylsilyl)phosphido}carbonylnitrosyl(pentamethylcyclopentadienyl)rhenium
CAS No.:111960-38-4
Molecular Formula:C₁₇H₃₃NO₂PReSi₂
Molecular Weight:556.806
Hs Code.:

Synonyms:{bis(trimethylsilyl)phosphido}carbonylnitrosyl(pentamethylcyclopentadienyl)rhenium

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Chemical Property of {bis(trimethylsilyl)phosphido}carbonylnitrosyl(pentamethylcyclopentadienyl)rhenium

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Technology Process of {bis(trimethylsilyl)phosphido}carbonylnitrosyl(pentamethylcyclopentadienyl)rhenium

There total 1 articles about {bis(trimethylsilyl)phosphido}carbonylnitrosyl(pentamethylcyclopentadienyl)rhenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 111960-37-3
bromocarbonylnitrosyl(pentamethylcyclopentadienyl)rhenium

: 59624-91-8
LiP(Si(CH₃)3)2*2.8THF

: 111960-38-4
{bis(trimethylsilyl)phosphido}carbonylnitrosyl(pentamethylcyclopentadienyl)rhenium

: 15573-38-3
Tris(trimethylsilyl)phosphane

Guidance literature:: In Cyclopentane; under N2, addn. of Re-compound in 5 portions at 0°C, stirred at 20.degrree.C overnight; removal of volatiles in vac., dissolved in n-pentane, filtration, washed with n-pentane, fractd. crystn. at -28°C (filtrate); elem. anal.;

Reference yield:

: 111960-38-4
{bis(trimethylsilyl)phosphido}carbonylnitrosyl(pentamethylcyclopentadienyl)rhenium

: 79074-00-3
2,4,6-tri-t-butylphenylphosphonous dichloride

: 75-77-4
chloro-trimethyl-silane

: 111960-39-5
(η5-C5(CH3)5)(CO)(NO)RePP(2,4,6-tBu3C6H2)

Guidance literature:: In tetrahydrofuran; under N2, addn. of C6H2(C(CH3)3)3PCl2 at 0°C to a soln. of (C5(CH3)5)(CO)(NO)ReP(Si(CH3)3)2, stirred for 30 min at 0°C; not isolated, detected by (31)P-NMR and IR-spectroscopy;