[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)(mercapto)(methyl)germane

Base Information

Chemical Name:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)(mercapto)(methyl)germane
CAS No.:247245-81-4
Molecular Formula:C₄₃H₈₆GeSSi₆
Molecular Weight:876.325
Hs Code.:

Synonyms:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)(mercapto)(methyl)germane

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Chemical Property of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)(mercapto)(methyl)germane

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Technology Process of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)(mercapto)(methyl)germane

There total 4 articles about [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)(mercapto)(methyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 64-17-5
ethanol

: 152291-63-9
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germanethione

: 917-54-4
methyllithium

: 247245-81-4
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)(mercapto)(methyl)germane

Guidance literature:: In diethyl ether; -60°C, heating (to -20°C), warming ( room temp.); chromatography (SiO2, hexane); elem. anal.;
DOI:10.1021/ja991147x

Reference yield:

: 162088-75-7
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

: 247245-81-4
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)(mercapto)(methyl)germane

Guidance literature:: Multi-step reaction with 4 steps

1: LiC₁₀H₈ / tetrahydrofuran

3: hexane

4: diethyl ether

With LiC₁₀H₈; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/ja991147x