[1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide

Base Information

Chemical Name:[1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide
CAS No.:436863-80-8
Molecular Formula:C₁₂H₈N₆O₂S₂
Molecular Weight:332.367
Hs Code.:

[1,2,3]thiadiazole-4-carboxylic acid <i>N</i>'-phenyl-<i>N</i>'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide

Synonyms:[1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide

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Chemical Property of [1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide

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Technology Process of [1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide

There total 1 articles about [1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 4100-17-8
1,2,3-thiadiazole-4-carboxylic acid chloride

: 100-63-0
phenylhydrazine

: 436863-80-8
[1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide

Guidance literature:: DOI:10.1016/S0040-4039(01)02326-7

Reference yield: 30.0%

: 436863-80-8
[1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide

: 74-88-4
methyl iodide

: 5-methylsulfanyl-1-phenyl-pyrazolo[5,1-b][1,3]thiazine-2,7-dione

Guidance literature:: [1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide; With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 18h;

methyl iodide; In dimethyl sulfoxide;
DOI:10.1016/S0040-4039(01)02326-7

Reference yield: 25.0%

: 100-44-7
benzyl chloride

: 436863-80-8
[1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide

: 5-benzylsulfanyl-1-phenyl-pyrazolo[5,1-b][1,3]thiazine-2,7-dione

Guidance literature:: [1,2,3]thiadiazole-4-carboxylic acid N'-phenyl-N'-([1,2,3]thiadiazole-4-carbonyl)-hydrazide; With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 18h;

benzyl chloride; In dimethyl sulfoxide;
DOI:10.1016/S0040-4039(01)02326-7