dibutyl-p-styryltin chloride

Base Information

Chemical Name:dibutyl-p-styryltin chloride
CAS No.:74255-80-4
Molecular Formula:C₁₆H₂₅ClSn
Molecular Weight:371.537
Hs Code.:

Synonyms:dibutyl-p-styryltin chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibutyl-p-styryltin chloride

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Technology Process of dibutyl-p-styryltin chloride

There total 1 articles about dibutyl-p-styryltin chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.3%

: 1073-67-2,24991-47-7
4-vinylbenzyl chloride

: 683-18-1
dibutyltin chloride

: 7439-95-4
magnesium

: 74255-80-4
dibutyl-p-styryltin chloride

: 74255-79-1
di-n-butyl-di-p-vinylphenyltin

Guidance literature:: With t-butylcatechol; HCl; In tetrahydrofuran; byproducts: MgCl2; (Ar); Grignard soln. from Mg and styryl chloride was dropped to soln. of tin compd. within 1-1,5 h, t-butylcatechol was added and mixt. stirredovernight; THF was removed in vac., residue taken up in toluene and treated with dild. HCl (ice-cooling), org. phases were concd. and chromd. (silica gel,pentane/ether); 1st fraction yielded Bu2Sn(styryl)2; elem. anal.; 2nd fraction: Bu2Sn(styryl)Cl; elem. anal.;
DOI:10.1016/S0022-328X(00)93423-5

Reference yield: 94.0%

: 74255-80-4
dibutyl-p-styryltin chloride

: 42491-34-9
di-tert-butyl(trimethylsilyl)phosphane

: 75-77-4
chloro-trimethyl-silane

: 74333-50-9
dibutyl-p-styryltin di-t-butylphosphine

Guidance literature:: In diethyl ether; toluene; addn. of equimolar amts. of Me3SiP(t-Bu)2 in toluene to satd. soln. of (Bu)2(CH2CHPh)SnCl in ether, 1h, room temp., stirred, distn. under vac.,under Ar; elem. anal.;
DOI:10.1016/S0022-328X(00)82878-8