tert-butyl 6-(4-(1,3,2-dithiarsolan-2-yl)phenylamino)-6-oxohexylcarbamate

Base Information

Chemical Name:tert-butyl 6-(4-(1,3,2-dithiarsolan-2-yl)phenylamino)-6-oxohexylcarbamate
CAS No.:1334715-61-5
Molecular Formula:C₁₉H₂₉AsN₂O₃S₂
Molecular Weight:472.504
Hs Code.:

Synonyms:tert-butyl 6-(4-(1,3,2-dithiarsolan-2-yl)phenylamino)-6-oxohexylcarbamate

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Chemical Property of tert-butyl 6-(4-(1,3,2-dithiarsolan-2-yl)phenylamino)-6-oxohexylcarbamate

Chemical Property:

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Technology Process of tert-butyl 6-(4-(1,3,2-dithiarsolan-2-yl)phenylamino)-6-oxohexylcarbamate

There total 4 articles about tert-butyl 6-(4-(1,3,2-dithiarsolan-2-yl)phenylamino)-6-oxohexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 6404-29-1
6-(tert-butoxycarbonylamino)hexanoic acid

: 5577-20-8
4-(1,3,2-dithiocycloarsenic-2-yl)aniline

: 1334715-61-5
tert-butyl 6-(4-(1,3,2-dithiarsolan-2-yl)phenylamino)-6-oxohexylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201101317

Reference yield:

: 98-50-0
p-aminophenylarsonic acid

: 1334715-61-5
tert-butyl 6-(4-(1,3,2-dithiarsolan-2-yl)phenylamino)-6-oxohexylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: phenylhydrazine / methanol / 1.17 h / Reflux

2: ethanol / 0.17 h / Reflux

3: N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; phenylhydrazine; HATU; In tetrahydrofuran; methanol; ethanol;
DOI:10.1002/anie.201101317

Reference yield:

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 1334715-61-5
tert-butyl 6-(4-(1,3,2-dithiarsolan-2-yl)phenylamino)-6-oxohexylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water; 1,4-dioxane / 3 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / tetrahydrofuran; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201300567