methyl 3-(2-(diethylamino)-2-hydroxyethyl)-5-(5-methylpyridin-2-yl)benzoate

Base Information

Chemical Name:methyl 3-(2-(diethylamino)-2-hydroxyethyl)-5-(5-methylpyridin-2-yl)benzoate
CAS No.:1186519-36-7
Molecular Formula:C₂₀H₂₆N₂O₃
Molecular Weight:342.438
Hs Code.:

Synonyms:methyl 3-(2-(diethylamino)-2-hydroxyethyl)-5-(5-methylpyridin-2-yl)benzoate

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Chemical Property of methyl 3-(2-(diethylamino)-2-hydroxyethyl)-5-(5-methylpyridin-2-yl)benzoate

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Technology Process of methyl 3-(2-(diethylamino)-2-hydroxyethyl)-5-(5-methylpyridin-2-yl)benzoate

There total 5 articles about methyl 3-(2-(diethylamino)-2-hydroxyethyl)-5-(5-methylpyridin-2-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 307353-32-8
3-bromo-5-hydroxymethylbenzoic acid methyl ester

: 1186519-36-7
methyl 3-(2-(diethylamino)-2-hydroxyethyl)-5-(5-methylpyridin-2-yl)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: manganese(IV) oxide / dichloromethane / 20 °C

2.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere; warming

2.2: 0.33 h / 0 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

4.1: ethanol / 50 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

With manganese(IV) oxide; n-butyllithium; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; toluene;

Reference yield:

: 1186519-96-9
methyl 3-bromo-5-vinylbenzoate

: 1186519-36-7
methyl 3-(2-(diethylamino)-2-hydroxyethyl)-5-(5-methylpyridin-2-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

2: ethanol / 50 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

With 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; toluene;

Reference yield:

: 51760-21-5
dimethyl 5-bromoisophthalate

: 1186519-36-7
methyl 3-(2-(diethylamino)-2-hydroxyethyl)-5-(5-methylpyridin-2-yl)benzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / methanol / 0 - 20 °C

2.1: manganese(IV) oxide / dichloromethane / 20 °C

3.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere; warming

3.2: 0.33 h / 0 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

5.1: ethanol / 50 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

With manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; toluene;