3-[ethoxycarbonyl(methoxycarbonyl)methyl]-2-methyl-3-phenylisoindolin-1-one

Base Information

Chemical Name:3-[ethoxycarbonyl(methoxycarbonyl)methyl]-2-methyl-3-phenylisoindolin-1-one
CAS No.:1449378-84-0
Molecular Formula:C₂₁H₂₁NO₅
Molecular Weight:367.401
Hs Code.:

Synonyms:3-[ethoxycarbonyl(methoxycarbonyl)methyl]-2-methyl-3-phenylisoindolin-1-one

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Chemical Property of 3-[ethoxycarbonyl(methoxycarbonyl)methyl]-2-methyl-3-phenylisoindolin-1-one

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Technology Process of 3-[ethoxycarbonyl(methoxycarbonyl)methyl]-2-methyl-3-phenylisoindolin-1-one

There total 7 articles about 3-[ethoxycarbonyl(methoxycarbonyl)methyl]-2-methyl-3-phenylisoindolin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 64-17-5
ethanol

: 201230-82-2
carbon monoxide

: 1449378-57-7
CF₃O₃S^(1-)*C₂₄H₃₂N₃O₃Pd⁽¹⁺⁾

: 1236158-28-3
dimethylaminoethyldimethylammonium trifluoromethanesulfonate

: 1449378-84-0
3-[ethoxycarbonyl(methoxycarbonyl)methyl]-2-methyl-3-phenylisoindolin-1-one

Guidance literature:: In chloroform; at 20 ℃; for 6h; under 1050.11 Torr;
DOI:10.1021/om4006406

Reference yield: 97.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 1449378-59-9
CF₃O₃S^(1-)*C₂₅H₃₄N₃O₃Pd⁽¹⁺⁾

: 1236158-28-3
dimethylaminoethyldimethylammonium trifluoromethanesulfonate

: 1449378-84-0
3-[ethoxycarbonyl(methoxycarbonyl)methyl]-2-methyl-3-phenylisoindolin-1-one

Guidance literature:: In chloroform; at 20 ℃; for 6h; under 1050.11 Torr;
DOI:10.1021/om4006406

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 1449378-84-0
3-[ethoxycarbonyl(methoxycarbonyl)methyl]-2-methyl-3-phenylisoindolin-1-one

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / dichloromethane / 6 h / 50 °C / Inert atmosphere

2: water / 0 °C / Inert atmosphere

3: dichloromethane / 1.5 h / 20 °C / Inert atmosphere

4: acetone / 0.5 h / 20 °C

5: dichloromethane / 48 h / 20 °C

6: chloroform / 6 h / 20 °C / 1050.11 Torr

With thionyl chloride; In dichloromethane; chloroform; water; acetone;
DOI:10.1021/om4006406