(R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester

Base Information

Chemical Name:(R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester
CAS No.:208253-69-4
Molecular Formula:C₂₃H₃₁NO₃Si
Molecular Weight:397.59
Hs Code.:

Synonyms:(R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester

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Chemical Property of (R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester

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Technology Process of (R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester

There total 1 articles about (R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 218766-08-6
(R)-2-(Benzhydrylidene-amino)-3-hydroxy-propionic acid methyl ester

: 208253-69-4
(R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1021/jo980951j

Reference yield: 72.0%

: 17049-50-2
n-decyl magnesium bromide

: 208253-69-4
(R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester

: 377082-50-3
(2R,3R)-2-(benhydrylideneamino)-1-(tert-butyldimethylsilanyloxy)tridecan-3-ol

: (2R,3S)-2-(benzhydrylideneamino)-1-(tert-butyldimethylsilanyloxy)tridecan-3-ol

Guidance literature:: (R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester; With i-Bu₂AlH*i-Bu₃Al; In hexane; dichloromethane; at -78 ℃; for 0.75h;

n-decyl magnesium bromide; In diethyl ether; hexane; dichloromethane; at -78 - 20 ℃;
DOI:10.1021/jo015844v

Reference yield: 65.6%

: 78887-70-4
pentadecylmagnesium bromide

: 208253-69-4
(R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester

: (2R,3R)-2-(benzhydrylideneamino)-1-(tert-butyldimethylsilanyloxy)octadecan-3-ol

: (2R,3S)-2-(benzhydrylideneamino)-1-(tert-butyldimethylsilanyloxy)octadecan-3-ol

Guidance literature:: (R)-2-(Benzhydrylidene-amino)-3-(tert-butyl-dimethyl-silanyloxy)-propionic acid methyl ester; With i-Bu₂AlH*i-Bu₃Al; In hexane; dichloromethane; at -78 ℃; for 0.75h;

pentadecylmagnesium bromide; In diethyl ether; hexane; dichloromethane; at -78 - 20 ℃;
DOI:10.1021/jo015844v