3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester

Base Information

• Chemical Name: 3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester
• CAS No.: 117227-45-9
• Molecular Formula: C₁₃H₁₅N₃O₄
• Molecular Weight: 277.28

Synonyms:3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester

Chemical Property of 3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester

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Technology Process of 3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester

There total 7 articles about 3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

3-Methyl-4-{[1-phenyl-meth-(E)-ylidene]-amino}-4H-cyclopenta[1,2,4]triazine-5,7-dicarboxylic acid diethyl ester (117227-40-4) → benzaldehyde (100-52-7) + benzonitrile (100-47-0) + 3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester (117227-45-9)

Guidance literature:

With sodium methylate; In ethanol; for 3h; Product distribution; Heating;

Reference yield: 66.0%

4-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-3-methyl-4,6-dihydro-1H-cyclopenta[1,2,4]triazine-5,7-dicarboxylic acid diethyl ester (117227-22-2) → 4-methoxy-benzaldehyde (123-11-5) + 4-methoxybenzonitrile (874-90-8) + 3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester (117227-45-9)

Guidance literature:

With ethanol; Heating;

Reference yield: 65.0%

4-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-3-methyl-4H-cyclopenta[1,2,4]triazine-5,7-dicarboxylic acid diethyl ester (117227-42-6) → 4-methoxy-benzaldehyde (123-11-5) + 4-methoxybenzonitrile (874-90-8) + 3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester (117227-45-9)

Guidance literature:

With sodium methylate; In ethanol; for 3h; Product distribution; Heating;

upstream raw materials:

3-nitro-benzaldehyde

4-Amino-4,6-dihydro-3-methyl-1H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester

benzaldehyde

3-Methyl-4-{[1-phenyl-meth-(E)-ylidene]-amino}-4H-cyclopenta[1,2,4]triazine-5,7-dicarboxylic acid diethyl ester

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