(1,4,7,10,13-pentaoxa-cyclohexadec-15-ylmethyl)-triphenylstannane

Base Information

Chemical Name:(1,4,7,10,13-pentaoxa-cyclohexadec-15-ylmethyl)-triphenylstannane
CAS No.:948052-79-7
Molecular Formula:C₃₀H₃₈O₅Sn
Molecular Weight:597.339
Hs Code.:

Synonyms:(1,4,7,10,13-pentaoxa-cyclohexadec-15-ylmethyl)-triphenylstannane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1,4,7,10,13-pentaoxa-cyclohexadec-15-ylmethyl)-triphenylstannane

Chemical Property:

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Technology Process of (1,4,7,10,13-pentaoxa-cyclohexadec-15-ylmethyl)-triphenylstannane

There total 1 articles about (1,4,7,10,13-pentaoxa-cyclohexadec-15-ylmethyl)-triphenylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 69496-18-0
15-methylene-1,4,7,10,13-pentaoxacyclohexadecane

: 892-20-6
triphenylstannane

: 948052-79-7
(1,4,7,10,13-pentaoxa-cyclohexadec-15-ylmethyl)-triphenylstannane

Guidance literature:: With aibn; In dichloromethane; addn. of 15-methylene-1,4,7,10,13-pentaoxacyclohexadecane and aibn to Ph3SnH; stirring at 70°C for 12 h; cooling to room temp., addn. of CH2Cl2; filtration through Celite; removal of solvent in vac., chromy. with silica gel and CH2Cl2; elution with EtOH; elem. anal.;
DOI:10.1021/om700304p

Reference yield: 99.0%

: 948052-79-7
(1,4,7,10,13-pentaoxa-cyclohexadec-15-ylmethyl)-triphenylstannane

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 948052-80-0
iodo(1,4,7,10,13-pentaoxacyclohexadec-15-ylmethyl)diphenylstannane

Guidance literature:: In dichloromethane; byproducts: iodobenzene; addn. in small portions under ice of I2 (1 equiv.) to stirred soln. of (1,4,7,10,13-pentaoxacyclohexadec-15-ylmethyl)triphenylstannane (1 equiv.) in CH2Cl2; stirring overnight; removal of solvent and the iodobenzene in vac.; addn. of CH2Cl2, filtration, evapn. of solvent; crystn., elem. anal.;
DOI:10.1021/om700304p

Reference yield: 98.0%

: 75-09-2
dichloromethane

: 948052-79-7
(1,4,7,10,13-pentaoxa-cyclohexadec-15-ylmethyl)-triphenylstannane

: 7726-95-6
bromine

: bromo(1,4,7,10,13-pentaoxacyclohexadec-15-ylmethyl)diphenylstannane dichloromethane hemisolvate

Guidance literature:: In dichloromethane; byproducts: C6H5Br; addn. dropwise of Br2 in CH2Cl2 to cooled (-55°C) soln. of (1,4,7,10,13-pentaoxacyclohexadec-15-ylmethyl)triphenylstannane in CH2Cl2; warming to room temp. overnight; removal of volatiles in vac.; recrystn. from EtOH; elem. anal.;
DOI:10.1021/om700304p