2,2-dimethyl-10-(2,2-diphenylethyl)-4,7,11-trioxo-3,12-dioxa-5,10-diazapentadec-14-ene

Base Information

• Chemical Name: 2,2-dimethyl-10-(2,2-diphenylethyl)-4,7,11-trioxo-3,12-dioxa-5,10-diazapentadec-14-ene
• CAS No.: 1185841-59-1
• Molecular Formula: C₂₇H₃₄N₂O₅
• Molecular Weight: 466.577

Synonyms:2,2-dimethyl-10-(2,2-diphenylethyl)-4,7,11-trioxo-3,12-dioxa-5,10-diazapentadec-14-ene

Chemical Property of 2,2-dimethyl-10-(2,2-diphenylethyl)-4,7,11-trioxo-3,12-dioxa-5,10-diazapentadec-14-ene

Chemical Property:

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Technology Process of 2,2-dimethyl-10-(2,2-diphenylethyl)-4,7,11-trioxo-3,12-dioxa-5,10-diazapentadec-14-ene

There total 5 articles about 2,2-dimethyl-10-(2,2-diphenylethyl)-4,7,11-trioxo-3,12-dioxa-5,10-diazapentadec-14-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

tert-butyl 4-(2,2-diphenylethylamino)-2-oxobutylcarbamate (1185653-21-7) + Allyl chloroformate (2937-50-0) → 2,2-dimethyl-10-(2,2-diphenylethyl)-4,7,11-trioxo-3,12-dioxa-5,10-diazapentadec-14-ene (1185841-59-1)

Guidance literature:

Reference yield:

BOC-glycine (4530-20-5) → 2,2-dimethyl-10-(2,2-diphenylethyl)-4,7,11-trioxo-3,12-dioxa-5,10-diazapentadec-14-ene (1185841-59-1)

Guidance literature:

Multi-step reaction with 4 steps

1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

2: tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3: dichloromethane / 2 h / 20 °C

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

(2-oxobut-3-enyl)carbamic acid tert-butyl ester (121505-96-2) → 2,2-dimethyl-10-(2,2-diphenylethyl)-4,7,11-trioxo-3,12-dioxa-5,10-diazapentadec-14-ene (1185841-59-1)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 2 h / 20 °C

In dichloromethane;

upstream raw materials:

tert-butyl 4-(2,2-diphenylethylamino)-2-oxobutylcarbamate

Allyl chloroformate

BOC-glycine

2,2-Diphenylethylamine

Downstream raw materials:

(2R)-allyl 5-(benzyloxycarbonylamino)-2-(10-(2,2-diphenylethyl)-2,2-dimethyl-4,11-dioxo-3,12-dioxa-5,10-diazapentadec-14-en-7-ylamino)pentanoate

(3R,5R)-5-(N-Boc-aminomethyl)-3-(N-Cbz-3-aminopropyl)-1-(2,2-diphenylethyl)-1,4-diazepan-2-one

(3R,5S)-5-(N-Boc-aminomethyl)-3-(N-Cbz-3-aminopropyl)-1-(2,2-diphenylethyl)-1,4-diazepan-2-one

(3R,5S)-5-(N-Boc-aminomethyl)-3-(N,N'-Cbz₂-3-guanidinopropyl)-1-(2,2-diphenylethyl)-1,4-diazepan-2-one

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