d₅-acetophenone O-methyloxime

Base Information

Chemical Name:d₅-acetophenone O-methyloxime
CAS No.:1352619-55-6
Molecular Formula:C₉H₁₁NO
Molecular Weight:154.153
Hs Code.:

d<SUB>5</SUB>-acetophenone O-methyloxime

Synonyms:d₅-acetophenone O-methyloxime

Suppliers and Price of d₅-acetophenone O-methyloxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of d₅-acetophenone O-methyloxime

Chemical Property:

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Technology Process of d₅-acetophenone O-methyloxime

There total 1 articles about d₅-acetophenone O-methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28077-64-7
acetophenone-d5

: 593-56-6
N-methoxylamine hydrochloride

: 1352619-55-6
d₅-acetophenone O-methyloxime

Guidance literature:: In methanol; water; for 18h; Reflux;
DOI:10.1021/ol203046n

Reference yield: 65.0%

: 1352619-55-6
d₅-acetophenone O-methyloxime

: 458532-84-8
2-chloro-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pyridine

: C₁₄H₉⁽²⁾H₄ClN₂O

Guidance literature:: With tris(acetonitrile)pentamethylcyclopentadienylrhodium(III) hexafluoroantimonate; lithium fluoride; silver(l) oxide; In chlorobenzene; at 100 ℃; for 5h; Time; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1039/d1ob02201f

Reference yield: 39.0%

: 1352619-55-6
d₅-acetophenone O-methyloxime

: 100-52-7
benzaldehyde

: C₁₆H₁₁⁽²⁾H₄NO₂

Guidance literature:: With N-hydroxyphthalimide; oxygen; palladium diacetate; In 1,4-dioxane; at 80 ℃; for 1h; under 760.051 Torr; Time; Schlenk technique;
DOI:10.1039/c5cc08945j