C₄₁H₅₃N₇O₁₀S

Base Information

Chemical Name:C₄₁H₅₃N₇O₁₀S
CAS No.:274901-51-8
Molecular Formula:C₄₁H₅₃N₇O₁₀S
Molecular Weight:835.979
Hs Code.:

C<sub>41</sub>H<sub>53</sub>N<sub>7</sub>O<sub>10</sub>S

Synonyms:C₄₁H₅₃N₇O₁₀S

Suppliers and Price of C₄₁H₅₃N₇O₁₀S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₁H₅₃N₇O₁₀S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₁H₅₃N₇O₁₀S

There total 13 articles about C₄₁H₅₃N₇O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2480-93-5
Boc-Orn(Z)-OH

: 274901-51-8
C₄₁H₅₃N₇O₁₀S

Guidance literature:: Multi-step reaction with 12 steps

1.1: ethyl chloroformate / tetrahydrofuran / 0.25 h / -10 - 0 °C

1.2: 83 percent / NaBH₄ / tetrahydrofuran; methanol / 0 °C

2.1: 80 percent / triethylamine / CH₂Cl₂ / 1.5 h / 0 - 20 °C

3.1: 69 percent / Cs₂CO₃ / dimethylformamide / 0 °C

4.1: sulfuryl chloride; acetic anhydride / CH₂Cl₂ / 1 h / -20 - -5 °C

5.1: 73 percent / NH₃ / CH₂Cl₂ / 0.25 h / -10 °C

6.1: 85 percent / NaIO₄ / RuCl₃*H₂O / CH₂Cl₂; acetonitrile; H₂O / 0.75 h / 0 - 20 °C

7.1: hydrogen / 10percent Pd/C / ethanol / 4 h

8.1: 230 mg / tetrahydrofuran

9.1: TFA / CH₂Cl₂ / 0.5 h / 0 °C

10.1: 81 mg / BOP; DIPEA / CH₂Cl₂

11.1: TFA / CH₂Cl₂ / 0.5 h / 0 °C

12.1: 68 mg / BOP; DIPEA / CH₂Cl₂

With sodium periodate; sulfuryl dichloride; ammonia; hydrogen; chloroformic acid ethyl ester; acetic anhydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; ruthenium trichloride; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1.1: Substitution / 1.2: Reduction / 2.1: Substitution / 3.1: Substitution / 4.1: Deacetylation / 5.1: Substitution / 6.1: Oxidation / 7.1: Hydrogenolysis / 8.1: Substitution / 9.1: Hydrolysis / 10.1: Condensation / 11.1: Hydrolysis / 12.1: Condensation;
DOI:10.1002/1099-0690(200004)2000:7<1219::AID-EJOC1219>3.0.CO;2-P

Reference yield:

: 105562-75-2
N²-(tert-butyloxycarbonyl)-N⁵-(benzyloxycarbonyl)-2(S),5-diaminopentanol

: 274901-51-8
C₄₁H₅₃N₇O₁₀S

Guidance literature:: Multi-step reaction with 11 steps

1: 80 percent / triethylamine / CH₂Cl₂ / 1.5 h / 0 - 20 °C

2: 69 percent / Cs₂CO₃ / dimethylformamide / 0 °C

3: sulfuryl chloride; acetic anhydride / CH₂Cl₂ / 1 h / -20 - -5 °C

4: 73 percent / NH₃ / CH₂Cl₂ / 0.25 h / -10 °C

5: 85 percent / NaIO₄ / RuCl₃*H₂O / CH₂Cl₂; acetonitrile; H₂O / 0.75 h / 0 - 20 °C

6: hydrogen / 10percent Pd/C / ethanol / 4 h

7: 230 mg / tetrahydrofuran

8: TFA / CH₂Cl₂ / 0.5 h / 0 °C

9: 81 mg / BOP; DIPEA / CH₂Cl₂

10: TFA / CH₂Cl₂ / 0.5 h / 0 °C

11: 68 mg / BOP; DIPEA / CH₂Cl₂

With sodium periodate; sulfuryl dichloride; ammonia; hydrogen; acetic anhydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; ruthenium trichloride; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1: Substitution / 2: Substitution / 3: Deacetylation / 4: Substitution / 5: Oxidation / 6: Hydrogenolysis / 7: Substitution / 8: Hydrolysis / 9: Condensation / 10: Hydrolysis / 11: Condensation;
DOI:10.1002/1099-0690(200004)2000:7<1219::AID-EJOC1219>3.0.CO;2-P

Reference yield:

: 233689-90-2
Boc-NH-CH((CH₂)3NHZ)-CH₂-S-CO-CH₃

: 274901-51-8
C₄₁H₅₃N₇O₁₀S

Guidance literature:: Multi-step reaction with 9 steps

1: sulfuryl chloride; acetic anhydride / CH₂Cl₂ / 1 h / -20 - -5 °C

2: 73 percent / NH₃ / CH₂Cl₂ / 0.25 h / -10 °C

3: 85 percent / NaIO₄ / RuCl₃*H₂O / CH₂Cl₂; acetonitrile; H₂O / 0.75 h / 0 - 20 °C

4: hydrogen / 10percent Pd/C / ethanol / 4 h

5: 230 mg / tetrahydrofuran

6: TFA / CH₂Cl₂ / 0.5 h / 0 °C

7: 81 mg / BOP; DIPEA / CH₂Cl₂

8: TFA / CH₂Cl₂ / 0.5 h / 0 °C

9: 68 mg / BOP; DIPEA / CH₂Cl₂

With sodium periodate; sulfuryl dichloride; ammonia; hydrogen; acetic anhydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; ruthenium trichloride; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile; 1: Deacetylation / 2: Substitution / 3: Oxidation / 4: Hydrogenolysis / 5: Substitution / 6: Hydrolysis / 7: Condensation / 8: Hydrolysis / 9: Condensation;
DOI:10.1002/1099-0690(200004)2000:7<1219::AID-EJOC1219>3.0.CO;2-P