5'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine

Base Information

Chemical Name:5'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine
CAS No.:76991-44-1
Molecular Formula:C₂₉H₃₅N₅O₁₀
Molecular Weight:613.624
Hs Code.:

Synonyms:5'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine

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Chemical Property of 5'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine

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Technology Process of 5'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine

There total 1 articles about 5'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 71874-01-6
3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine

: 123-76-2
levulinic acid

: 76991-44-1
5'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine

: 76998-99-7
2'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; 2-chloro-1-methyl-pyridinium iodide; In 1,4-dioxane; acetonitrile; for 2h;
DOI:10.1021/jo00324a010

Reference yield: 86.0%

: 59819-52-2
2,2,2-trichloroethyl 2-chlorophenyl phosphorochloridate

: 76991-44-1
5'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine

: 76991-45-2
5'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine 2'-O-(2-chlorophenyl 2,2,2-trichloroethyl phosphate)

Guidance literature:: With 1-methyl-1H-imidazole; In acetonitrile; at 0 ℃; for 0.75h;
DOI:10.1021/jo00324a010

Reference yield:

: 76991-44-1
5'-O-levulinyl-3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine

: 76991-46-3
3'-O-(4-methoxytetrahydropyran-4-yl)-6-N-p-anisoyladenosine 2'-O-(2-chlorophenyl 2,2,2-trichloroethyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / 1-methylimidazole / acetonitrile / 0.75 h / 0 °C

2: 92 percent / hydrazine hydrate / pyridine; acetic acid / 0.07 h / Ambient temperature

With 1-methyl-1H-imidazole; hydrazine hydrate; In pyridine; acetic acid; acetonitrile;
DOI:10.1021/jo00324a010