(3-METHOXYPHENOXY) ACETIC ACID ETHYL ESTER

Base Information

• Chemical Name: (3-METHOXYPHENOXY) ACETIC ACID ETHYL ESTER
• CAS No.: 82815-86-9
• Molecular Formula: C11H14 O4
• Molecular Weight: 210.23
• Hs Code.: 2918990090
• Mol file: 82815-86-9.mol

Synonyms:Aceticacid, (3-methoxyphenoxy)-, ethyl ester (9CI); Acetic acid, (m-methoxyphenoxy)-,ethyl ester (6CI,7CI); 3-Methoxyphenoxyacetic acid ethyl ester; Ethyl(3-methoxyphenoxy)acetate

Chemical Property of (3-METHOXYPHENOXY) ACETIC ACID ETHYL ESTER

Chemical Property:

• PSA: 44.76000
• LogP: 1.63710

Purity/Quality:

98%min ^*data from raw suppliers

ethyl2-(3-methoxyphenoxy)acetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-METHOXYPHENOXY) ACETIC ACID ETHYL ESTER

There total 7 articles about (3-METHOXYPHENOXY) ACETIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

O-methylresorcine (150-19-6) + chloroacetic acid ethyl ester (105-39-5) → (3-methoxy-phenoxy)-acetic acid ethyl ester (82815-86-9)

Guidance literature:

O-methylresorcine; With potassium carbonate; potassium iodide; In water; acetone; Reflux; Large scale;

chloroacetic acid ethyl ester; In water; acetone; for 8h; Reflux; Large scale;

DOI:10.1021/acs.oprd.9b00546

Reference yield: 88.0%

ethanol (64-17-5) + 3-methoxyphenoxyacetic acid (2088-24-6) → (3-methoxy-phenoxy)-acetic acid ethyl ester (82815-86-9)

Guidance literature:

With toluene-4-sulfonic acid; at 20 ℃;

DOI:10.1007/s00044-009-9170-3

Reference yield: 76.0%

O-methylresorcine (150-19-6) + ethyl bromoacetate (105-36-2) → (3-methoxy-phenoxy)-acetic acid ethyl ester (82815-86-9)

Guidance literature:

With potassium carbonate; In acetone; at 20 ℃; for 24h; Reflux; Inert atmosphere;

DOI:10.1021/acs.orglett.5b00214

upstream raw materials:

ethanol

3-methoxyphenoxyacetic acid

O-methylresorcine

ethyl bromoacetate

Downstream raw materials:

3-methoxyphenoxyacetic acid

2-(3-methoxyphenoxy)acetamide

2-(3-methoxyphenoxy)acetylhydrazine

4-(3-methoxy-phenoxy)-acetoacetic acid ethyl ester