1-tert-butyl-5-methyl (2S,3S,1'R,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenylpentanedioate

Base Information

Chemical Name:1-tert-butyl-5-methyl (2S,3S,1'R,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenylpentanedioate
CAS No.:942220-63-5
Molecular Formula:C₃₈H₄₃NO₄
Molecular Weight:577.764
Hs Code.:

Synonyms:1-tert-butyl-5-methyl (2S,3S,1'R,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenylpentanedioate

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Chemical Property of 1-tert-butyl-5-methyl (2S,3S,1'R,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenylpentanedioate

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Technology Process of 1-tert-butyl-5-methyl (2S,3S,1'R,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenylpentanedioate

There total 6 articles about 1-tert-butyl-5-methyl (2S,3S,1'R,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenylpentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 67-56-1
methanol

: tert-butyl (2S,3S,1'R,4''S,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenyl-5-oxo-5-(4''-phenyl-5'',5''-dimethyl-oxazolidin-2''-one-3''-yl)pentanoate

: 942220-63-5
1-tert-butyl-5-methyl (2S,3S,1'R,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenylpentanedioate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1039/b701226h

Reference yield: 56.0%

: 67-56-1
methanol

: tert-butyl (1'R,4''S,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenyl-5-oxo-5-(4''-benzyl-oxazolidin-2''-one-3''-yl)pentanoate

: tert-butyl (2S,3S,1'R,1''S,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenyl-4-(1''-benzyl-2''-hydroxyethylcarbamoyl)butanoate

: 942220-63-5
1-tert-butyl-5-methyl (2S,3S,1'R,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenylpentanedioate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1039/b701226h

Reference yield: 15.0%

: 103-26-4,1754-62-7
methyl cinnamate

: 265669-72-5
tert-butyl (3R,αS)-3-[N-benzyl-N-(α-methylbenzyl)amino]-3-phenylpropanoate

: 942220-63-5
1-tert-butyl-5-methyl (2S,3S,1'R,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenylpentanedioate

: 1,7-di-tert-butyl (2S,3S,1'R,αS)-2-[1'-phenyl-1'-(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenyl-5-oxoheptanedioate

Guidance literature:: tert-butyl (3R,αS)-3-[N-benzyl-N-(α-methylbenzyl)amino]-3-phenylpropanoate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 - 0 ℃; for 0.666667h;

methyl cinnamate; In tetrahydrofuran; at -78 - 0 ℃; for 2h; Further stages.;
DOI:10.1039/b701226h