[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]⁽¹⁺⁾*BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]BF₄

Base Information

Chemical Name:[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]⁽¹⁺⁾*BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]BF₄
CAS No.:284472-96-4
Molecular Formula:BF₄*C₄₆H₄₁N₆P₂Ru
Molecular Weight:927.694
Hs Code.:

[(CH(C<sub>3</sub>H<sub>3</sub>N<sub>2</sub>)3)Ru(P(C<sub>6</sub>H<sub>5</sub>)3)2H]<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=[(CH(C<sub>3</sub>H<sub>3</sub>N<sub>2</sub>)3)Ru(P(C<sub>6</sub>H<sub>5</sub>)3)2H]BF<sub>4</sub>

Synonyms:[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]⁽¹⁺⁾*BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]BF₄

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Chemical Property of [(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]⁽¹⁺⁾*BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]BF₄

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Technology Process of [(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]⁽¹⁺⁾*BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]BF₄

There total 1 articles about [(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]⁽¹⁺⁾*BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 55102-19-7
hydridochlorotris(triphenylphosphine)ruthenium(II)

: 13755-29-8
sodium tetrafluoroborate

: 80510-03-8
Tris(pyrazolyl)methane

: 284472-96-4
[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]⁽¹⁺⁾*BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]BF₄

Guidance literature:: In tetrahydrofuran; under N2; stirring soln. of RuHCl(PPh3)3, tris(1-pyrazolyl)methane and NaBF4 in THF at room temp. for 1 h; evapn. under vac., washing with MeOH, recrystn. from CH2Cl2/hexane; elem. anal.;
DOI:10.1002/(SICI)1099-0682(200005)2000:5<993::AID-EJIC993>3.0.CO;2-3

Reference yield: 88.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 284472-96-4
[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]⁽¹⁺⁾*BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]BF₄

: 7732-18-5
water

: [(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2(H₂O)]⁽²⁺⁾*2BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2(H₂O)](BF₄)2

: 1333-74-0
hydrogen

Guidance literature:: In dichloromethane; under N2; addn. of excess HBF4*Et2O followed by H2O to soln. of Ru complex in CH2Cl2, stirring at room temp. for 30 min; evapn. under vac., washing with Et2O; elem. anal.;
DOI:10.1002/(SICI)1099-0682(200005)2000:5<993::AID-EJIC993>3.0.CO;2-3

Reference yield:

: 284472-96-4
[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]⁽¹⁺⁾*BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2H]BF₄

: DBF₄

: [(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2(H⁽²⁾H)]⁽²⁺⁾*2BF₄^(1-)=[(CH(C₃H₃N₂)3)Ru(P(C₆H₅)3)2(H⁽²⁾H)](BF₄)2

Guidance literature:: In dichloromethane-d2; under N2; addn. of DBF4 to soln. of Ru complex in CD2Cl2 at -50°C; not isolated; NMR;
DOI:10.1002/(SICI)1099-0682(200005)2000:5<993::AID-EJIC993>3.0.CO;2-3