Technology Process of benzyl 5-(chloromethyl)-2,3-dihydro-1H-inden-1-ylcarbamate
There total 6 articles about benzyl 5-(chloromethyl)-2,3-dihydro-1H-inden-1-ylcarbamate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
thionyl chloride;
In
dichloromethane;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / water; ethyl acetate
2: 1,8-diazabicyclo[5.4.0]undec-7-ene; tri tert-butylphosphoniumtetrafluoroborate; molybdenum hexacarbonyl / methanol; acetonitrile / 0.5 h / 150 °C / Irradiation with microwave
3: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C
4: thionyl chloride / dichloromethane / 2 h / 20 °C
With
lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; tri tert-butylphosphoniumtetrafluoroborate; molybdenum hexacarbonyl;
In
tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; tri tert-butylphosphoniumtetrafluoroborate; molybdenum hexacarbonyl / methanol; acetonitrile / 0.5 h / 150 °C / Irradiation with microwave
2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C
3: thionyl chloride / dichloromethane / 2 h / 20 °C
With
lithium aluminium tetrahydride; thionyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; tri tert-butylphosphoniumtetrafluoroborate; molybdenum hexacarbonyl;
In
tetrahydrofuran; methanol; dichloromethane; acetonitrile;