5-(1-adamantyl)-4-benzyloxy-2-methoxyphenyl bromide

Base Information

Chemical Name:5-(1-adamantyl)-4-benzyloxy-2-methoxyphenyl bromide
CAS No.:1313053-10-9
Molecular Formula:C₂₄H₂₇BrO₂
Molecular Weight:427.381
Hs Code.:

Synonyms:5-(1-adamantyl)-4-benzyloxy-2-methoxyphenyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(1-adamantyl)-4-benzyloxy-2-methoxyphenyl bromide

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Technology Process of 5-(1-adamantyl)-4-benzyloxy-2-methoxyphenyl bromide

There total 3 articles about 5-(1-adamantyl)-4-benzyloxy-2-methoxyphenyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1313053-09-6
2-(1-adamantyl)-4-bromo-5-methoxyphenol

: 100-39-0
benzyl bromide

: 1313053-10-9
5-(1-adamantyl)-4-benzyloxy-2-methoxyphenyl bromide

Guidance literature:: With potassium carbonate; In acetone; for 17.25h; Reflux; Inert atmosphere;

Reference yield:

: 768-95-6
1-adamanthanol

: 1313053-10-9
5-(1-adamantyl)-4-benzyloxy-2-methoxyphenyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonic acid / dichloromethane / 29 h / 54 °C

2: potassium carbonate / acetone / 17.25 h / Reflux; Inert atmosphere

With methanesulfonic acid; potassium carbonate; In dichloromethane; acetone;

Reference yield:

: 102127-34-4
4-bromo-3-methoxyphenol

: 1313053-10-9
5-(1-adamantyl)-4-benzyloxy-2-methoxyphenyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonic acid / dichloromethane / 29 h / 54 °C

2: potassium carbonate / acetone / 17.25 h / Reflux; Inert atmosphere

With methanesulfonic acid; potassium carbonate; In dichloromethane; acetone;