9-(1-Methyl-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-ylamino)-9-oxononanoic acid

Base Information

Chemical Name:9-(1-Methyl-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-ylamino)-9-oxononanoic acid
CAS No.:1449305-58-1
Molecular Formula:C₂₅H₂₉N₃O₄
Molecular Weight:435.523
Hs Code.:

Synonyms:9-(1-Methyl-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-ylamino)-9-oxononanoic acid

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Chemical Property of 9-(1-Methyl-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-ylamino)-9-oxononanoic acid

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Technology Process of 9-(1-Methyl-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-ylamino)-9-oxononanoic acid

There total 4 articles about 9-(1-Methyl-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-ylamino)-9-oxononanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: C₂₇H₃₃N₃O₄

: 1449305-58-1
9-(1-Methyl-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-ylamino)-9-oxononanoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; for 2h;
DOI:10.1016/j.ejmech.2013.05.017

Reference yield:

: 103421-61-0
3-amino-1-methyl-5-phenyl-1,3-dihydro-2H-1,4-benzodiazepin-2-one

: 1449305-58-1
9-(1-Methyl-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-ylamino)-9-oxononanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol / chloroform / 18 h / 20 °C

2: sodium hydroxide / methanol; tetrahydrofuran; water / 2 h / 20 °C

With benzotriazol-1-ol; sodium hydroxide; In tetrahydrofuran; methanol; chloroform; water;
DOI:10.1016/j.ejmech.2013.05.017

Reference yield:

: 106849-47-2
1,3-dihydro-1-methyl-5-phenyl-3(R,S)-<(benzyloxycarbonyl)-amino>-2H-1,4-benzodiazepin-2-one

: 1449305-58-1
9-(1-Methyl-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-ylamino)-9-oxononanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen bromide / acetic acid / 2 h / 20 °C / Inert atmosphere

2: benzotriazol-1-ol / chloroform / 18 h / 20 °C

3: sodium hydroxide / methanol; tetrahydrofuran; water / 2 h / 20 °C

With hydrogen bromide; benzotriazol-1-ol; sodium hydroxide; In tetrahydrofuran; methanol; chloroform; water; acetic acid;
DOI:10.1016/j.ejmech.2013.05.017