(R)-2-methoxycarbonyl-3-phenylpentane-1,5-dioic acid 1,5-dimethyl ester

Base Information

Chemical Name:(R)-2-methoxycarbonyl-3-phenylpentane-1,5-dioic acid 1,5-dimethyl ester
CAS No.:222050-57-9
Molecular Formula:C₁₅H₁₈O₆
Molecular Weight:294.304
Hs Code.:

Synonyms:(R)-2-methoxycarbonyl-3-phenylpentane-1,5-dioic acid 1,5-dimethyl ester

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Chemical Property of (R)-2-methoxycarbonyl-3-phenylpentane-1,5-dioic acid 1,5-dimethyl ester

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Technology Process of (R)-2-methoxycarbonyl-3-phenylpentane-1,5-dioic acid 1,5-dimethyl ester

There total 12 articles about (R)-2-methoxycarbonyl-3-phenylpentane-1,5-dioic acid 1,5-dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 67-56-1
methanol

: 222050-34-2
(3R)-tert-butyl 4,4-dicarbomethoxy-3-phenylbutanethioate

: 222050-57-9
(R)-2-methoxycarbonyl-3-phenylpentane-1,5-dioic acid 1,5-dimethyl ester

Guidance literature:: With bromine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja002246+

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 108-59-8
malonic acid dimethyl ester

: 18107-18-1
diazomethyl-trimethyl-silane

: (S)-2-methyloxycarbonyl-3-phenylpentanedioic acid 1,5-dimethyl ester

: 222050-57-9
(R)-2-methoxycarbonyl-3-phenylpentane-1,5-dioic acid 1,5-dimethyl ester

Guidance literature:: (E)-3-phenylpropenal; malonic acid dimethyl ester; With (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; In ethanol; at 0 ℃; for 96h;

With potassium permanganate; sodium dihydrogenphosphate; In tert-butyl alcohol; for 0.0833333h;

diazomethyl-trimethyl-silane; In methanol; hexane; toluene; for 0.166667h; Title compound not separated from byproducts;
DOI:10.1002/anie.200601025

Reference yield:

: 860772-43-6
(E)-1-(1-methyl-1H-imidazole-2-yl)-3-phenylprop-2-en-1-one

: 67-56-1
methanol

: 108-59-8
malonic acid dimethyl ester

: (S)-2-methyloxycarbonyl-3-phenylpentanedioic acid 1,5-dimethyl ester

: 222050-57-9
(R)-2-methoxycarbonyl-3-phenylpentane-1,5-dioic acid 1,5-dimethyl ester

Guidance literature:: (E)-1-(1-methyl-1H-imidazole-2-yl)-3-phenylprop-2-en-1-one; malonic acid dimethyl ester; With salmon testes DNA; In water; acetonitrile; at 5 ℃; for 72h; pH=6.5;

With methyl trifluoromethanesulfonate; In acetonitrile; for 3h;

methanol; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; for 0.5h; Further stages. Title compound not separated from byproducts.;
DOI:10.1002/anie.200703459