methyl 2-(6-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)acetate

Base Information

Chemical Name:methyl 2-(6-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)acetate
CAS No.:1262008-23-0
Molecular Formula:C₂₈H₃₀F₃NO₄
Molecular Weight:501.546
Hs Code.:

Synonyms:methyl 2-(6-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)acetate

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Chemical Property of methyl 2-(6-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)acetate

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Technology Process of methyl 2-(6-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)acetate

There total 3 articles about methyl 2-(6-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1262008-05-8
2-(5-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1H-indol-3-yl)ethanol

: 105-45-3
acetoacetic acid methyl ester

: 1262008-23-0
methyl 2-(6-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)acetate

Guidance literature:: 2-(5-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1H-indol-3-yl)ethanol; acetoacetic acid methyl ester; toluene-4-sulfonic acid; In toluene; at 80 ℃; for 5h;

With sodium hydrogencarbonate; In toluene;

Reference yield:

: 154-02-9
5-hydroxytryptophol

: 1262008-23-0
methyl 2-(6-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C

2: toluene-4-sulfonic acid / toluene / 5 h / 80 °C

With caesium carbonate; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; toluene;

Reference yield:

: 957208-65-0
4-(chloromethyl)-1-cyclopentyl-2-(trifluoromethyl)benzene

: 1262008-23-0
methyl 2-(6-(4-cyclopentyl-3-(trifluoromethyl)benzyloxy)-1-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C

2: toluene-4-sulfonic acid / toluene / 5 h / 80 °C

With caesium carbonate; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; toluene;