ethyl N-salicylideneglycinate

Base Information

• Chemical Name: ethyl N-salicylideneglycinate
• CAS No.: 66949-73-3
• Molecular Formula: C₁₁H₁₃NO₃
• Molecular Weight: 207.229

Synonyms:ethyl N-salicylideneglycinate

Chemical Property of ethyl N-salicylideneglycinate

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of ethyl N-salicylideneglycinate

There total 3 articles about ethyl N-salicylideneglycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

glycine ethyl ester hydrochloride (623-33-6) + salicylaldehyde (90-02-8) → ethyl N-salicylideneglycinate (66949-73-3)

Guidance literature:

With ammonia; In diethyl ether; 1.) 1 h, 2.) reflux, 1 h;

DOI:10.1080/00397919908086261

Reference yield:

copper(II) bis(salicylaldehyde) + GlyOEt*HCl (459-73-4) → ethyl N-salicylideneglycinate (66949-73-3)

Guidance literature:

In ethanol;

DOI:10.1246/bcsj.42.1297

Reference yield:

→ ethyl N-salicylideneglycinate (66949-73-3)

Guidance literature:

Aethylglycinat, Salicylaldehyd (auf chromatogr. Platten, S. 168/170);

upstream raw materials:

GlyOEt*HCl

glycine ethyl ester hydrochloride

salicylaldehyde

Downstream raw materials:

N-(benzyl)salicylaldimine

aminocoumarine

N-(2-hydroxybenzyl)glycine ethyl ester

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