5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine

Base Information

Chemical Name:5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine
CAS No.:1237587-85-7
Molecular Formula:C₁₆H₁₁Cl₃F₃N₃O
Molecular Weight:424.637
Hs Code.:

Synonyms:5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine

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Chemical Property of 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine

Chemical Property:

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Technology Process of 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine

There total 5 articles about 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1071927-85-9
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chloroaniline

: 1237587-85-7
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine

Guidance literature:: 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chloroaniline; With hydrogenchloride; sodium nitrite; In 1,4-dioxane; water; at 0 ℃;

With hydrogenchloride; tin(ll) chloride; In 1,4-dioxane; water;

With sodium hydroxide; In 1,4-dioxane; water;

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 1237587-85-7
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid; iron / ethanol / 0.83 h / 75 °C

3.1: hydrogenchloride / 1,4-dioxane / 0.33 h / 20 °C

3.2: 0.25 h / 0 °C

With hydrogenchloride; N-chloro-succinimide; water; iron; acetic acid; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 66399-01-7
2-chloro-5-hydroxyiminomethylnitrobenzene

: 1237587-85-7
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid; iron / ethanol / 0.83 h / 75 °C

3.1: hydrogenchloride / 1,4-dioxane / 0.33 h / 20 °C

3.2: 0.25 h / 0 °C

With hydrogenchloride; N-chloro-succinimide; water; iron; acetic acid; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;