C₁₅H₂₀ClNO₃

Base Information

Chemical Name:C₁₅H₂₀ClNO₃
CAS No.:1403595-91-4
Molecular Formula:C₁₅H₂₀ClNO₃
Molecular Weight:297.782
Hs Code.:

C<sub>15</sub>H<sub>20</sub>ClNO<sub>3</sub>

Synonyms:C₁₅H₂₀ClNO₃

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Chemical Property of C₁₅H₂₀ClNO₃

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Technology Process of C₁₅H₂₀ClNO₃

There total 7 articles about C₁₅H₂₀ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1403595-90-3
methyl 5-chloro-3-(ethyl (tetrahydro-2H-pyran-4-yl) amino)-2-methylbenzoate

: 1403595-91-4
C₁₅H₂₀ClNO₃

Guidance literature:: methyl 5-chloro-3-(ethyl (tetrahydro-2H-pyran-4-yl) amino)-2-methylbenzoate; With water; sodium hydroxide; In ethanol; at 60 ℃; for 1h;

With hydrogenchloride; citric acid; In water; pH=4 - 6;

Reference yield:

: 7499-06-1
5-chloro-2-methylbenzoic acid

: 1403595-91-4
C₁₅H₂₀ClNO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / 0.17 h / -10 °C

1.2: 0.5 h / -10 °C

2.1: sodium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

3.1: water; ammonium chloride; iron / ethanol / 1 h / 80 °C

4.1: acetic acid / methanol / 3 h / 20 °C

5.1: caesium carbonate / acetonitrile / 18 h / 80 °C

6.1: sodium hydroxide; water / ethanol / 1 h / 60 °C

6.2: pH 4 - 6

With sulfuric acid; water; iron; sodium carbonate; ammonium chloride; caesium carbonate; acetic acid; sodium hydroxide; In methanol; ethanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 294190-17-3
methyl 5-chloro-2-methyl-3-nitrobenzoate

: 1403595-91-4
C₁₅H₂₀ClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; ammonium chloride; iron / ethanol / 1 h / 80 °C

2.1: acetic acid / methanol / 3 h / 20 °C

3.1: caesium carbonate / acetonitrile / 18 h / 80 °C

4.1: sodium hydroxide; water / ethanol / 1 h / 60 °C

4.2: pH 4 - 6

With water; iron; ammonium chloride; caesium carbonate; acetic acid; sodium hydroxide; In methanol; ethanol; acetonitrile;