1-benzyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.1(3,7)]decane bromide

Base Information

• Chemical Name: 1-benzyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.1(3,7)]decane bromide
• CAS No.: 1234455-26-5
• Molecular Formula: Br*C₁₃H₁₉N₃P
• Molecular Weight: 328.192
• Mol file: 1234455-26-5.mol

Synonyms:1-benzyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.1(3,7)]decane bromide

Chemical Property of 1-benzyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.1(3,7)]decane bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-benzyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.1(3,7)]decane bromide

There total 1 articles about 1-benzyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.1(3,7)]decane bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

benzyl bromide (100-39-0) + (1,3,5-triaza-7-phosphaadamantane) (53597-69-6) → 1-benzyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.1(3,7)]decane bromide (1234455-26-5)

Guidance literature:

In acetone; at 0 ℃; for 0.416667h; Inert atmosphere;

DOI:10.1016/j.poly.2010.03.012

Reference yield: 84.0%

1-benzyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.1(3,7)]decane bromide (1234455-26-5) + [Au(C6F5)(tetrahydrothiophene)] → [Au(C6F5)(1,3,5-triaza-7-phosphaadamantane-CH2Ph)]Br (1431464-09-3)

Guidance literature:

In acetone; for 4h;

DOI:10.1002/ejic.201201411

Reference yield: 76.0%

1-benzyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.1(3,7)]decane bromide (1234455-26-5) + [Au2{μ-2-C6H4P(S)Ph2}2] → [Au(PTA-CH2Ph){κC-2-C6H4P(S)Ph2}]Br

Guidance literature:

In dichloromethane;

upstream raw materials:

benzyl bromide

(1,3,5-triaza-7-phosphaadamantane)

Downstream raw materials:

(1-benzyl-3,5-diaza-1-azonia-7-phosphatricyclo[3.3.1.1(3,7)]decane-P)gold(I) bromide chloride

[Au(C₆F₅)(1,3,5-triaza-7-phosphaadamantane-CH₂Ph)]Br