dimethyl p-chlorophenoxyisobutyrylphosphonate

Base Information

• Chemical Name: dimethyl p-chlorophenoxyisobutyrylphosphonate
• CAS No.: 81928-53-2
• Molecular Formula: C₁₂H₁₆ClO₅P
• Molecular Weight: 306.683

Synonyms:dimethyl p-chlorophenoxyisobutyrylphosphonate

Chemical Property of dimethyl p-chlorophenoxyisobutyrylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dimethyl p-chlorophenoxyisobutyrylphosphonate

There total 2 articles about dimethyl p-chlorophenoxyisobutyrylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Clofibrate (637-07-0) → dimethyl p-chlorophenoxyisobutyrylphosphonate (81928-53-2)

Guidance literature:

With phosphorous acid trimethyl ester; In thionyl chloride;

Reference yield:

clofibryl chloride (5542-60-9) + phosphorous acid trimethyl ester (121-45-9) → dimethyl p-chlorophenoxyisobutyrylphosphonate (81928-53-2)

Guidance literature:

Ambient temperature;

DOI:10.1021/jm00391a027

Reference yield: 66.0%

Dimethyl phosphite (868-85-9) + dimethyl p-chlorophenoxyisobutyrylphosphonate (81928-53-2) → [2-(4-Chloro-phenoxy)-1-(dimethoxy-phosphoryl)-1-hydroxy-2-methyl-propyl]-phosphonic acid dimethyl ester

Guidance literature:

With dibutylamine; In diethyl ether; at 0 ℃; for 1h;

DOI:10.1021/jm00391a027

upstream raw materials:

clofibryl chloride

phosphorous acid trimethyl ester

Clofibrate

Downstream raw materials:

clofibryl chloride

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