{t-butyl(trimethylsilyl)amino}(diisopropylamino)fluoroborane

Base Information

Chemical Name:{t-butyl(trimethylsilyl)amino}(diisopropylamino)fluoroborane
CAS No.:112794-84-0
Molecular Formula:C₁₃H₃₂BFN₂Si
Molecular Weight:274.305
Hs Code.:

Synonyms:{t-butyl(trimethylsilyl)amino}(diisopropylamino)fluoroborane

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Chemical Property of {t-butyl(trimethylsilyl)amino}(diisopropylamino)fluoroborane

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Technology Process of {t-butyl(trimethylsilyl)amino}(diisopropylamino)fluoroborane

There total 1 articles about {t-butyl(trimethylsilyl)amino}(diisopropylamino)fluoroborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 109-72-8,29786-93-4
n-butyllithium

: 5577-67-3
trimethyl(tert-butylamino)silane

: 109-63-7
trifluoroborane diethyl ether

: 108-18-9
diisopropylamine

: lithium tetrafluoroborate

: 112794-84-0
{t-butyl(trimethylsilyl)amino}(diisopropylamino)fluoroborane

: 7789-24-4
lithium fluoride

Guidance literature:: In diethyl ether; hexane; n-BuLi in hexane added to i-Pr2NH in Et2O at 0°C; mixt. stirred for 1 h at room temp., then cooled to 0°C; BF3*Et2O added dropwise; soln. refluxed for 6 h; LiBF4 filtered off; t-Bu(SiMe3)NH in Et2O and n-BuLi in hexane added; volatile compounds removed in vac.; vac. distn.; elem. anal.;

Reference yield: 83.0%

: 112794-84-0
{t-butyl(trimethylsilyl)amino}(diisopropylamino)fluoroborane

: 118331-75-2
(t-butylimino)(diisopropylamino)borane

: 118331-77-4
1,3-di-t-butyl-2,4-bis(diisopropylamino)-1,3,2,4-diazadiboretidine

: 420-56-4
trimethylsilyl fluoride

Guidance literature:: In hexane; products of the thermal decompn. of (i-Pr2N)BFN(t-Bu)SiMe3 at 560°C and 0.02 Torr are dissolved in pentane at -78°C; soln. stirred at room temp. for 12 h; ppt. filtered, washed with pentane, dried in vac.; elem. anal.;