[8-(4-benzyloxy-2,6-dimethoxyphenyl)-2,7-dimethylpyrazolo[1,5-a][1,3,5]triazin-4-yl]bis(2-methoxyethyl)amine

Base Information

Chemical Name:[8-(4-benzyloxy-2,6-dimethoxyphenyl)-2,7-dimethylpyrazolo[1,5-a][1,3,5]triazin-4-yl]bis(2-methoxyethyl)amine
CAS No.:1217490-66-8
Molecular Formula:C₂₈H₃₅N₅O₅
Molecular Weight:521.616
Hs Code.:

Synonyms:[8-(4-benzyloxy-2,6-dimethoxyphenyl)-2,7-dimethylpyrazolo[1,5-a][1,3,5]triazin-4-yl]bis(2-methoxyethyl)amine

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Chemical Property of [8-(4-benzyloxy-2,6-dimethoxyphenyl)-2,7-dimethylpyrazolo[1,5-a][1,3,5]triazin-4-yl]bis(2-methoxyethyl)amine

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Technology Process of [8-(4-benzyloxy-2,6-dimethoxyphenyl)-2,7-dimethylpyrazolo[1,5-a][1,3,5]triazin-4-yl]bis(2-methoxyethyl)amine

There total 6 articles about [8-(4-benzyloxy-2,6-dimethoxyphenyl)-2,7-dimethylpyrazolo[1,5-a][1,3,5]triazin-4-yl]bis(2-methoxyethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 111-95-5
Bis-(2-methoxyethyl)amine

: 1217490-63-5
8-(4-benzyloxy-2,6-dimethoxyphenyl)-4-chloro-2,7-dimethylpyrazolo[1,5-a][1,3,5]triazine

: 1217490-66-8
[8-(4-benzyloxy-2,6-dimethoxyphenyl)-2,7-dimethylpyrazolo[1,5-a][1,3,5]triazin-4-yl]bis(2-methoxyethyl)amine

Guidance literature:: In tetrahydrofuran; for 1h;
DOI:10.1002/jlcr.1616

Reference yield:

: 22080-96-2
syringaldehyde

: 1217490-66-8
[8-(4-benzyloxy-2,6-dimethoxyphenyl)-2,7-dimethylpyrazolo[1,5-a][1,3,5]triazin-4-yl]bis(2-methoxyethyl)amine

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / acetone / 14 h / Reflux

2: potassium tert-butylate / 1,2-dimethoxyethane / 3 h / -60 - -50 °C

3: sodium / 1.83 h / Reflux

4: hydrazine hydrate; acetic acid / toluene / 5 h / Reflux

5: acetonitrile / 18 h / 20 °C

6: sodium ethanolate / ethanol / 6 h / Reflux

7: N,N-diethyl-p-toluidine; trichlorophosphate / 24 h / Reflux

8: tetrahydrofuran / 1 h

With N,N-diethyl-p-toluidine; potassium tert-butylate; sodium ethanolate; sodium; potassium carbonate; hydrazine hydrate; acetic acid; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; acetone; toluene; acetonitrile;
DOI:10.1002/jlcr.1616

Reference yield:

: 679428-14-9
1-benzyloxy-4-formyl-3,5-dimethoxybenzene

: 1217490-66-8
[8-(4-benzyloxy-2,6-dimethoxyphenyl)-2,7-dimethylpyrazolo[1,5-a][1,3,5]triazin-4-yl]bis(2-methoxyethyl)amine

Guidance literature:: Multi-step reaction with 7 steps

1: potassium tert-butylate / 1,2-dimethoxyethane / 3 h / -60 - -50 °C

2: sodium / 1.83 h / Reflux

3: hydrazine hydrate; acetic acid / toluene / 5 h / Reflux

4: acetonitrile / 18 h / 20 °C

5: sodium ethanolate / ethanol / 6 h / Reflux

6: N,N-diethyl-p-toluidine; trichlorophosphate / 24 h / Reflux

7: tetrahydrofuran / 1 h

With N,N-diethyl-p-toluidine; potassium tert-butylate; sodium ethanolate; sodium; hydrazine hydrate; acetic acid; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; toluene; acetonitrile;
DOI:10.1002/jlcr.1616