2-({4-[2-(4-chlorophenyl)-1-(5-methyl-4H-1,2,4-triazol-3-yl)ethenyl]phenoxy}methyl)imidazo[1,2-a]pyridine

Base Information

Chemical Name:2-({4-[2-(4-chlorophenyl)-1-(5-methyl-4H-1,2,4-triazol-3-yl)ethenyl]phenoxy}methyl)imidazo[1,2-a]pyridine
CAS No.:1346569-40-1
Molecular Formula:C₂₅H₂₀ClN₅O
Molecular Weight:441.92
Hs Code.:

Synonyms:2-({4-[2-(4-chlorophenyl)-1-(5-methyl-4H-1,2,4-triazol-3-yl)ethenyl]phenoxy}methyl)imidazo[1,2-a]pyridine

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Chemical Property of 2-({4-[2-(4-chlorophenyl)-1-(5-methyl-4H-1,2,4-triazol-3-yl)ethenyl]phenoxy}methyl)imidazo[1,2-a]pyridine

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Technology Process of 2-({4-[2-(4-chlorophenyl)-1-(5-methyl-4H-1,2,4-triazol-3-yl)ethenyl]phenoxy}methyl)imidazo[1,2-a]pyridine

There total 9 articles about 2-({4-[2-(4-chlorophenyl)-1-(5-methyl-4H-1,2,4-triazol-3-yl)ethenyl]phenoxy}methyl)imidazo[1,2-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1346570-36-2
3-(4-chlorophenyl)-2-[4-(imidazo[1,2-a]pyridin-2-ylmethoxy)phenyl]prop-2-enehydrazide

: 124-42-5
acetamidine hydrochloride

: 1346569-40-1
2-({4-[2-(4-chlorophenyl)-1-(5-methyl-4H-1,2,4-triazol-3-yl)ethenyl]phenoxy}methyl)imidazo[1,2-a]pyridine

Guidance literature:: With sodium ethanolate; In ethanol; for 16h; Reflux;

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1346569-40-1
2-({4-[2-(4-chlorophenyl)-1-(5-methyl-4H-1,2,4-triazol-3-yl)ethenyl]phenoxy}methyl)imidazo[1,2-a]pyridine

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / 3 h / Reflux

1.2: 0.5 h / Reflux

2.1: sulfuric acid / 16 h / Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 60 °C

4.1: sodium hydroxide; water / ethanol / 16 h / 22 - 26 °C

5.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5.2: 1 h / 0 - 10 °C / Inert atmosphere

6.1: sodium ethanolate / ethanol / 16 h / Reflux

With sulfuric acid; water; sodium ethanolate; chloroformic acid ethyl ester; potassium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; 1.1: Perkin Reaction;

Reference yield:

: 504-29-0
2-aminopyridine

: 1346569-40-1
2-({4-[2-(4-chlorophenyl)-1-(5-methyl-4H-1,2,4-triazol-3-yl)ethenyl]phenoxy}methyl)imidazo[1,2-a]pyridine

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1,2-dimethoxyethane

2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 60 °C

3.1: sodium hydroxide; water / ethanol / 16 h / 22 - 26 °C

4.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

4.2: 1 h / 0 - 10 °C / Inert atmosphere

5.1: sodium ethanolate / ethanol / 16 h / Reflux

With water; sodium ethanolate; chloroformic acid ethyl ester; potassium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; N,N-dimethyl-formamide;