N,N-Dimethyl-2-phenylcyclopropaneamide

Base Information

Chemical Name:N,N-Dimethyl-2-phenylcyclopropaneamide
CAS No.:93085-87-1
Molecular Formula:C₁₂H₁₅NO
Molecular Weight:189.257
Hs Code.:

Synonyms:N,N-Dimethyl-2-phenylcyclopropaneamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-Dimethyl-2-phenylcyclopropaneamide

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Technology Process of N,N-Dimethyl-2-phenylcyclopropaneamide

There total 8 articles about N,N-Dimethyl-2-phenylcyclopropaneamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 23020-15-7
(1S,2S)-2-phenylcyclopropane-1-carboxylic acid

: 124-40-3
dimethyl amine

: 5279-83-4,35682-53-2,93085-87-1
(1S*,2S*)-N,N-dimethyl-2-phenylcyclopropane-1-carboxamide

Guidance literature:: (1S,2S)-2-phenylcyclopropane-1-carboxylic acid; With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 23 ℃; for 2h;

dimethyl amine; In dichloromethane; water; N,N-dimethyl-formamide; at 0 - 23 ℃; for 2h;
DOI:10.1002/anie.201900233

Reference yield: 82.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 62285-47-6
2-diazo-N,N-dimethyl-acetamide

: 100-52-7
benzaldehyde

: 5279-83-4,35682-53-2,93085-87-1
(1R*,2R*)-N,N-dimethyl-2-phenylcyclopropanecarboxamide

Guidance literature:: 2-diazo-N,N-dimethyl-acetamide; benzaldehyde; With copper(l) iodide; triphenylphosphine; In toluene; at 80 ℃; Inert atmosphere;

diazomethane; With palladium diacetate; In toluene; at -78 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/b810708d