allyl-3,4-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Base Information

• Chemical Name: allyl-3,4-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside
• CAS No.: 287922-85-4
• Molecular Formula: C₂₆H₃₀Cl₃NO₇
• Molecular Weight: 574.886

Synonyms:allyl-3,4-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Chemical Property of allyl-3,4-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of allyl-3,4-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

There total 3 articles about allyl-3,4-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

allyl 3-O-benzyl-4,6-O-benzylidene-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside (287922-84-3) → allyl-3,4-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside (287922-85-4)

Guidance literature:

With dimethylamine borane; boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃;

DOI:10.1055/s-2006-958410

Reference yield:

benzyl bromide (100-39-0) → allyl-3,4-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside (287922-85-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / Ag₂O

2: 86 percent / BH₃*Me₂NH; BF₃*OEt₂ / CH₂Cl₂

With dimethylamine borane; boron trifluoride diethyl etherate; silver(l) oxide; In dichloromethane; 1: benzylation / 2: Reduction;

DOI:10.1016/S0040-4039(00)01158-8

Reference yield:

allyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside (183388-21-8) → allyl-3,4-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside (287922-85-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / Ag₂O

2: 86 percent / BH₃*Me₂NH; BF₃*OEt₂ / CH₂Cl₂

With dimethylamine borane; boron trifluoride diethyl etherate; silver(l) oxide; In dichloromethane; 1: benzylation / 2: Reduction;

DOI:10.1016/S0040-4039(00)01158-8

upstream raw materials:

allyl 3-O-benzyl-4,6-O-benzylidene-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

benzyl bromide

allyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Downstream raw materials:

((2S,3R,4R,5S,6R)-2-Allyloxy-4,5-bis-benzyloxy-6-benzyloxymethoxymethyl-tetrahydro-pyran-3-yl)-carbamic acid 2,2,2-trichloro-ethyl ester

C₅₈H₆₄Cl₃NO₁₄

(R)-3-(4-Trifluoromethyl-benzyloxy)-octadecanoic acid ((2S,3R,4R,5S,6R)-2-allyloxy-4,5-bis-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-amide

2,2,2-Trichloro-acetimidic acid (3R,4R,5S,6R)-4,5-bis-benzyloxy-6-benzyloxymethoxymethyl-3-(2,2,2-trichloro-ethoxycarbonylamino)-tetrahydro-pyran-2-yl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 287922-85-4 allyl-3,4-di-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send