S-phenyl benzenethiosulfinate

Base Information

Chemical Name:S-phenyl benzenethiosulfinate
CAS No.:4409-79-4
Molecular Formula:C₁₂H₁₀OS₂
Molecular Weight:234.343
Hs Code.:

Synonyms:S-phenyl benzenethiosulfinate

Suppliers and Price of S-phenyl benzenethiosulfinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-phenyl benzenethiosulfinate

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Technology Process of S-phenyl benzenethiosulfinate

There total 9 articles about S-phenyl benzenethiosulfinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 67-56-1
methanol

: 135197-83-0
phenyl-3,4-O-diacetyl-2,6-dideoxy-1-thio-α-L-galactopyranoside

: 78464-95-6
methyl 3,4-di-O-acetyl-2,6-dideoxy-α-L-lyxo-hexopyranoside

: 4409-79-4
S-phenyl benzenethiosulfinate

Guidance literature:: methanol; phenyl-3,4-O-diacetyl-2,6-dideoxy-1-thio-α-L-galactopyranoside; With polymer-bound I(OTs)OH^(1-); In dichloromethane; at 20 ℃; for 24h;

With Amberlyst A-21; In dichloromethane; for 0.5h;

With borohydride exchange resin; In isopropyl alcohol; at 20 ℃; for 12h;
DOI:10.1016/S0040-4039(02)02708-9

Reference yield: 90.0%

: 54815-45-1
ethyl benzenesulfenate

: 4409-79-4
S-phenyl benzenethiosulfinate

Guidance literature:: With iodide; In water; at 25 ℃; Rate constant;
DOI:10.1016/S0040-4039(00)94418-6

Reference yield: 84.0%

: 20031-21-4
1,2-O-isopropylidene-α-D-xylose

: 135197-83-0
phenyl-3,4-O-diacetyl-2,6-dideoxy-1-thio-α-L-galactopyranoside

: 4409-79-4
S-phenyl benzenethiosulfinate

: Acetic acid (2S,3R,4S,6R)-3-acetoxy-6-((3aR,5R,6S,6aR)-6-hydroxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethoxy)-2-methyl-tetrahydro-pyran-4-yl ester

Guidance literature:: 1,2-O-isopropylidene-α-D-xylose; phenyl-3,4-O-diacetyl-2,6-dideoxy-1-thio-α-L-galactopyranoside; With polymer-bound I(OTs)OH^(1-); In dichloromethane; at 40 ℃; for 24h;

With Amberlyst A-21; In dichloromethane; for 0.5h;

With borohydride exchange resin; In isopropyl alcohol; at 20 ℃; for 12h;
DOI:10.1016/S0040-4039(02)02708-9