tert-butyl pyridine-3-carboxylate

Base Information

Chemical Name:tert-butyl pyridine-3-carboxylate
CAS No.:65321-36-0
Molecular Formula:C10H13 N O2
Molecular Weight:179.219
Hs Code.:

Synonyms:Nicotinicacid, tert-butyl ester (6CI,7CI); 1,1-Dimethylethyl nicotinate; tert-Butyl3-pyridinecarboxylate; tert-Butyl nicotinate

Suppliers and Price of tert-butyl pyridine-3-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of tert-butyl pyridine-3-carboxylate

Chemical Property:

Vapor Pressure:0.0399mmHg at 25°C
Boiling Point:239.5°C at 760 mmHg
Flash Point:98.7°C
Density:1.053g/cm³

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-butyl pyridine-3-carboxylate

There total 12 articles about tert-butyl pyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 329214-79-1
3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

: 65321-36-0
t-butyl nicotinate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In 1,4-dioxane; at 80 ℃; for 12h; Reagent/catalyst; Solvent; Time; Catalytic behavior; Inert atmosphere; Green chemistry;
DOI:10.1039/c4gc02443e

Reference yield: 84.0%

: 93-60-7
methyl 3-pyridinecarboxylate

: 75-65-0
tert-butyl alcohol

: 65321-36-0
t-butyl nicotinate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; for 1h;
DOI:10.1039/c39860000695

Reference yield: 68.0%

: 626-55-1,163928-56-1
3-Bromopyridine

: 201230-82-2
carbon monoxide

: 865-48-5
sodium t-butanolate

: 65321-36-0
t-butyl nicotinate

Guidance literature:: With 1,1'-bis(diisopropylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; at 70 ℃; Inert atmosphere;
DOI:10.1021/ol203057w