5-chloro-2,3-dimethoxyphenylmethanol

Base Information

Chemical Name:5-chloro-2,3-dimethoxyphenylmethanol
CAS No.:86232-35-1
Molecular Formula:C₉H₁₁ClO₃
Molecular Weight:202.638
Hs Code.:

Synonyms:5-chloro-2,3-dimethoxyphenylmethanol

Suppliers and Price of 5-chloro-2,3-dimethoxyphenylmethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 5-chloro-2,3-dimethoxyphenylmethanol

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-chloro-2,3-dimethoxyphenylmethanol

There total 4 articles about 5-chloro-2,3-dimethoxyphenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 86232-28-2
5-chloro-2,3-dimethoxybenzaldehyde

: 86232-35-1
5-chloro-2,3-dimethoxyphenylmethanol

Guidance literature:: With methanol; C₂₅H₂₉ClNO₂Rh; caesium carbonate; at 90 ℃; for 1h;
DOI:10.1039/c8cc06612d

Reference yield:

: 7740-05-8
5-chloro-2-hydroxy-3-methoxy-benzaldehyde

: 86232-35-1
5-chloro-2,3-dimethoxyphenylmethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1) 99percent hydrazine hydrate, 2) KOH / 1) reflux, 5 h, 2) reflux, 5 h

2: 75 percent / K₂CO₃ / acetone / 5 h / Heating

3: 81 percent / NaBH₄ / propan-2-ol / 1 h / Heating

With potassium hydroxide; sodium tetrahydroborate; potassium carbonate; hydrazine hydrate; In isopropyl alcohol; acetone;

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 86232-35-1
5-chloro-2,3-dimethoxyphenylmethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 45 percent / chlorine / acetic acid / 5 h / 20 °C

2: 1) 99percent hydrazine hydrate, 2) KOH / 1) reflux, 5 h, 2) reflux, 5 h

3: 75 percent / K₂CO₃ / acetone / 5 h / Heating

4: 81 percent / NaBH₄ / propan-2-ol / 1 h / Heating

With potassium hydroxide; sodium tetrahydroborate; chlorine; potassium carbonate; hydrazine hydrate; In acetic acid; isopropyl alcohol; acetone;