Technology Process of 2,2,2',2'-Tetrachlor-1,1'-diphenyl-2,2'-trithiobis(ethanon)
There total 1 articles about 2,2,2',2'-Tetrachlor-1,1'-diphenyl-2,2'-trithiobis(ethanon) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; thionyl chloride;
for 48h;
Title compound not separated from byproducts;
Ambient temperature;
- Guidance literature:
-
acetophenone;
With
pyridine; thionyl chloride;
at 75 ℃;
for 6.5h;
2,2,2',2'-Tetrachlor-1,1'-diphenyl-2,2'-trithiobis(ethanon);
In
neat (no solvent);
at 140 ℃;
for 15h;
DOI:10.1021/acs.joc.5b01707
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethyl ether / -80 °C
2: CH3OC6H4PS4PC6H4OCH3 / toluene / 3 h / Heating
With
CH3OC6H4PS4PC6H4OCH3;
In
diethyl ether; toluene;