Benzoic acid, 2-amino-4-(1,1-dimethylethyl)-, methyl ester (9CI)

Base Information

Chemical Name:Benzoic acid, 2-amino-4-(1,1-dimethylethyl)-, methyl ester (9CI)
CAS No.:717879-44-2
Molecular Formula:C12H17 N O2
Molecular Weight:207.272
Hs Code.:
Mol file:717879-44-2.mol

Synonyms:Benzoic acid, 2-amino-4-(1,1-dimethylethyl)-, methyl ester (9CI)

Suppliers and Price of Benzoic acid, 2-amino-4-(1,1-dimethylethyl)-, methyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-AMINO-4-(1,1-DIMETHYLETHYL)-BENZOIC ACID METHYL ESTER 95.00%
5MG
$ 505.00

Total 0 raw suppliers

Chemical Property of Benzoic acid, 2-amino-4-(1,1-dimethylethyl)-, methyl ester (9CI)

Chemical Property:

Boiling Point:308.1±35.0 °C(Predicted)
PKA:2.44±0.10(Predicted)
PSA：52.32000
Density:1.055±0.06 g/cm3(Predicted)
LogP:2.93410

Purity/Quality:: 2-AMINO-4-(1,1-DIMETHYLETHYL)-BENZOIC ACID METHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Benzoic acid, 2-amino-4-(1,1-dimethylethyl)-, methyl ester (9CI)

There total 2 articles about Benzoic acid, 2-amino-4-(1,1-dimethylethyl)-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₁₆INO₂

: 717879-44-2
methyl 2-amino-4-tert-butylbenzoate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride; In 1,4-dioxane; at 85 ℃; for 18h;
DOI:10.1002/cmdc.201600467

Reference yield:

: 67-56-1
methanol

: 50727-07-6
4-tert-butylphthalimide

: 717879-44-2
methyl 2-amino-4-tert-butylbenzoate

: 1356116-19-2
methyl 4-tert-butyl-2-((methoxycarbonyl)amino)benzoate

: 1356116-23-8
methyl 5-tert-butyl-2-((methoxycarbonyl)amino)benzoate

Guidance literature:: methanol; With iodobenzene; toluene-4-sulfonic acid; sodium sulfate; 3-chloro-benzenecarboperoxoic acid; at 0 ℃; for 0.166667h; Inert atmosphere;

4-tert-butylphthalimide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 0 - 40 ℃; for 5h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol300028j

Reference yield: 47.0%

: 717879-44-2
methyl 2-amino-4-tert-butylbenzoate

: 939819-18-8
methyl 4-tert-butyl-2-fluorobenzoate

Guidance literature:: methyl 2-amino-4-tert-butylbenzoate; With boron trifluoride diethyl etherate; In 1,2-dimethoxyethane; at -10 ℃; for 0.5h;

With tert.-butylnitrite; In 1,2-dimethoxyethane; chlorobenzene; at -10 - 130 ℃; for 5h;