(4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)triphenylphosphonium chloride

Base Information

Chemical Name:(4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)triphenylphosphonium chloride
CAS No.:1311267-07-8
Molecular Formula:C₃₆H₃₁ClN₂O₂P*Cl
Molecular Weight:625.534
Hs Code.:

Synonyms:(4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)triphenylphosphonium chloride

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Chemical Property of (4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)triphenylphosphonium chloride

Chemical Property:

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Technology Process of (4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)triphenylphosphonium chloride

There total 1 articles about (4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)triphenylphosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.7%

: 1311267-00-1
3-(3-chloro-4-isopropoxyphenyl)-5-(4-(chloromethyl)phenyl)-1,2,4-oxadiazole

: 603-35-0
triphenylphosphine

: 1311267-07-8
(4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)triphenylphosphonium chloride

Guidance literature:: In xylene; at 140 ℃; for 18h;

Reference yield: 41.6%

: 1311267-07-8
(4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)triphenylphosphonium chloride

: 87121-89-9
ethyl 3-oxocyclobutanecarboxylate

: 1311229-08-9
ethyl 3-(4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzylidene)cyclobutanecarboxylate

Guidance literature:: (4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)triphenylphosphonium chloride; With sodium hydride; In dimethyl sulfoxide; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

ethyl 3-oxocyclobutanecarboxylate; In dimethyl sulfoxide; at 20 - 80 ℃; for 64.08h; Inert atmosphere;

Reference yield:

: 1311267-07-8
(4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)triphenylphosphonium chloride

: 1311231-88-5
3-(4-(3-(3-chloro-4-isopropoxyphenyl)-1,2,4-oxadiazol-5-yl)benzyl)cyclobutanecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / dimethyl sulfoxide / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 64.08 h / 20 - 80 °C / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1 h / 20 °C

3.1: potassium hydroxide; water / ethanol / 16 h / 100 °C

With water; hydrogen; sodium hydride; potassium hydroxide; palladium 10% on activated carbon; In ethanol; dimethyl sulfoxide; ethyl acetate;