2-phenylsulphonyl-2-trimethylsilyl oxirane

Base Information

Chemical Name:2-phenylsulphonyl-2-trimethylsilyl oxirane
CAS No.:148599-35-3
Molecular Formula:C₁₁H₁₆O₃SSi
Molecular Weight:256.398
Hs Code.:

Synonyms:2-phenylsulphonyl-2-trimethylsilyl oxirane

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Chemical Property of 2-phenylsulphonyl-2-trimethylsilyl oxirane

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Technology Process of 2-phenylsulphonyl-2-trimethylsilyl oxirane

There total 2 articles about 2-phenylsulphonyl-2-trimethylsilyl oxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75-77-4
chloro-trimethyl-silane

: 111832-37-2
2-(phenylsulfonyl)oxirane

: 148599-35-3
2-phenylsulphonyl-2-trimethylsilyl oxirane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -102 ℃;
DOI:10.1039/c39880000645

Reference yield:

: 7205-98-3
chloromethyl phenyl sulfone

: 148599-35-3
2-phenylsulphonyl-2-trimethylsilyl oxirane

Guidance literature:: Multi-step reaction with 2 steps

1: 50percent aq. NaOH, Et₃BnN(+)Br(-)

2: BuLi / tetrahydrofuran / -102 °C

With sodium hydroxide; n-butyllithium; benzyltriethylammonium bromide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)98809-9

Reference yield:

: 148599-35-3
2-phenylsulphonyl-2-trimethylsilyl oxirane

: 111832-37-2
2-(phenylsulfonyl)oxirane

Guidance literature:: With sodium hydride; phosphonic acid diethyl ester; Yield given. Multistep reaction; 1) THF, mineral oil, rt, 10 min, 2) THF, rt, 0.5 h;
DOI:10.1016/S0040-4039(00)60367-2