benzoic acid 4-(tert-butyl-dimethyl-silanyloxy)-2-(4-dimethylamino-2-methoxy-phenyl)-butyl ester

Base Information

Chemical Name:benzoic acid 4-(tert-butyl-dimethyl-silanyloxy)-2-(4-dimethylamino-2-methoxy-phenyl)-butyl ester
CAS No.:447461-93-0
Molecular Formula:C₂₆H₃₉NO₄Si
Molecular Weight:457.685
Hs Code.:

benzoic acid 4-(<i>tert</i>-butyl-dimethyl-silanyloxy)-2-(4-dimethylamino-2-methoxy-phenyl)-butyl ester

Synonyms:benzoic acid 4-(tert-butyl-dimethyl-silanyloxy)-2-(4-dimethylamino-2-methoxy-phenyl)-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoic acid 4-(tert-butyl-dimethyl-silanyloxy)-2-(4-dimethylamino-2-methoxy-phenyl)-butyl ester

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Technology Process of benzoic acid 4-(tert-butyl-dimethyl-silanyloxy)-2-(4-dimethylamino-2-methoxy-phenyl)-butyl ester

There total 4 articles about benzoic acid 4-(tert-butyl-dimethyl-silanyloxy)-2-(4-dimethylamino-2-methoxy-phenyl)-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 447461-92-9
(R)-4-benzoyloxy-3-(4-dimethylamino-2-methoxy-phenyl)-butyraldehyde

: 447461-93-0
benzoic acid 4-(tert-butyl-dimethyl-silanyloxy)-2-(4-dimethylamino-2-methoxy-phenyl)-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 303 mg / NaBH₄ / CH₂Cl₂; ethanol / 0.08 h

2: 400 mg / triethylamine; DMAP / CH₂Cl₂ / 1 h

With dmap; sodium tetrahydroborate; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/ja025981p

Reference yield:

: 15799-79-8
3-methoxy-N,N-dimethylaniline

: 447461-93-0
benzoic acid 4-(tert-butyl-dimethyl-silanyloxy)-2-(4-dimethylamino-2-methoxy-phenyl)-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: (2S,5S)-5-benzyl-2-tert-butyl-3-methyl-imidazolidinone; HCl / CHCl₃; dioxane / 24 h / -20 °C

2: 303 mg / NaBH₄ / CH₂Cl₂; ethanol / 0.08 h

3: 400 mg / triethylamine; DMAP / CH₂Cl₂ / 1 h

With hydrogenchloride; dmap; sodium tetrahydroborate; (2S,5S)-5-benzyl-2-tert-butyl-3-methyl-imidazolidinone; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; chloroform;
DOI:10.1021/ja025981p

Reference yield:

: 118017-13-3
trans-benzoic acid 4-oxo-but-2-enyl ester

: 447461-93-0
benzoic acid 4-(tert-butyl-dimethyl-silanyloxy)-2-(4-dimethylamino-2-methoxy-phenyl)-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: (2S,5S)-5-benzyl-2-tert-butyl-3-methyl-imidazolidinone; HCl / CHCl₃; dioxane / 24 h / -20 °C

2: 303 mg / NaBH₄ / CH₂Cl₂; ethanol / 0.08 h

3: 400 mg / triethylamine; DMAP / CH₂Cl₂ / 1 h

With hydrogenchloride; dmap; sodium tetrahydroborate; (2S,5S)-5-benzyl-2-tert-butyl-3-methyl-imidazolidinone; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; chloroform;
DOI:10.1021/ja025981p