6-phenoxydibenzo(1,3,2)-dioxaphosphepin 6-oxide

Base Information

Chemical Name:6-phenoxydibenzo(1,3,2)-dioxaphosphepin 6-oxide
CAS No.:105053-46-1
Molecular Formula:C₁₈H₁₃O₄P
Molecular Weight:324.273
Hs Code.:

6-phenoxydibenzo<d,f>(1,3,2)-dioxaphosphepin 6-oxide

Synonyms:6-phenoxydibenzo(1,3,2)-dioxaphosphepin 6-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-phenoxydibenzo(1,3,2)-dioxaphosphepin 6-oxide

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Technology Process of 6-phenoxydibenzo(1,3,2)-dioxaphosphepin 6-oxide

There total 5 articles about 6-phenoxydibenzo(1,3,2)-dioxaphosphepin 6-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1806-29-7
2,2'-dihydroxybiphenyl

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 105053-46-1
6-phenoxydibenzo(1,3,2)-dioxaphosphepin 6-oxide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 16h; Inert atmosphere; Sealed tube;
DOI:10.1055/s-0037-1611295

Reference yield: 77.0%

: 6-(1H-benzo[d][1,2,3]triazol-1-yl)dibenzo[d,f][1,3,2]dioxa phosphepine 6-oxide

: 108-95-2,27073-41-2
phenol

: 105053-46-1
6-phenoxydibenzo(1,3,2)-dioxaphosphepin 6-oxide

Guidance literature:: phenol; With triethylamine; for 0.0833333h;

6-(1H-benzo[d][1,2,3]triazol-1-yl)dibenzo[d,f][1,3,2]dioxa phosphepine 6-oxide; at 40 ℃; for 0.333333h; Microwave irradiation;
DOI:10.1016/j.tetlet.2014.07.057